119072-55-8合成路线 （共 225 条）
反应条件
1,3-bis-(diphenylphosphino)propane; caesium carbonate; palladium dichloride in toluene 16 h; Inert atmosphereReflux;
参考文献
Geden, Joanna V.; Pancholi, Alpa K.; Shipman, Michael
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4158 - 4164
反应条件
1,3-bis-(diphenylphosphino)propane; caesium carbonate; palladium dichloride in toluene 16 h; Inert atmosphereReflux;
参考文献
Geden, Joanna V.; Pancholi, Alpa K.; Shipman, Michael
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4158 - 4164
反应条件
in N,N-dimethyl-formamide T=120°C; 24 h; Inert atmosphere;
参考文献
Bochatay, Valentin N.; Boissarie, Patrick J.; Murphy, John A.; Suckling, Colin J.; Lang, Stuart
Journal of Organic Chemistry, 2013 , vol. 78, # 4 p. 1471 - 1477
反应条件
azodiisobutyric acid dinitrile in benzene byproducts: iso-C4H10; boiling for 24 h on reflux;;
参考文献
Saegusa et al.
Journal of the American Chemical Society, 1968 , vol. 90, p. 4182
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.5.4.8, page 63 - 65
反应条件
in dichloromethane 44 h; HeatingIrradiation;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 10 p. 2709 - 2714
反应条件
in acetone under inert gas; dropwise addn. of the isocyanide in acetone to the suspn. of the Pd complex in acetone in presence of NaBF4 at room temp.; stirring for 1 h; solvent removed, residue dissolved in CH2Cl2; soln. filtered and concd., addn. of Et2O yields the solid; elem. anal.;
参考文献
Michelin, Rino A.; Zanotto, Livio; Braga, Dario; Sabatino, Piera; Angelici, Robert J.
Inorganic Chemistry, 1988 , vol. 27, p. 85 - 92
反应条件
in deuterated toluene T=20°C; 5 h;
参考文献
Journal of the American Chemical Society, , vol. 134, # 6 p. 2954 - 2957
反应条件
triethylamine in acetonitrile
T=20°C; 24 h;
参考文献
Moderhack, Dietrich; Daoud, Ali
Journal of Heterocyclic Chemistry, 2003 , vol. 40, # 4 p. 625 - 637
反应条件
triethylamine in benzene
T=20°C; 24 h;
参考文献
Moderhack, Dietrich; Daoud, Ali
Journal of Heterocyclic Chemistry, 2003 , vol. 40, # 4 p. 625 - 637
反应条件
in hexane
molar ratio Ni(C8H12)2 : t-C4H9NC = 1 : 10;
参考文献
Nast, R.; Schulz, H.; Moerler, H.-D.
Chemische Berichte, 1970 , vol. 103, p. 777 - 784
Full Text Show Details
Gmelin Handbook: Ni: Org.Verb.1, 1.1.6.4.1, page 327 - 333
