119072-55-8合成路线 (共 225 条)
反应条件
in ammonia
react. in liq. NH3 at -33 - -40 °C;;
参考文献
Nast, R.; Schulz, H.; Moerler, H.-D.
Chemische Berichte, 1970 , vol. 103, p. 777 - 784
Full Text Show Details
Gmelin Handbook: Ni: Org.Verb.1, 1.1.6.4.1, page 327 - 333
反应条件
in toluene
byproducts: t-C4H9NCO; react. wirh excess t-C4H9NC in toluene at room temp.;;
参考文献
Nast, R.; Schulz, H.; Moerler, H.-D.
Chemische Berichte, 1970 , vol. 103, p. 777 - 784
Full Text Show Details
Gmelin Handbook: Ni: Org.Verb.1, 1.1.6.4.1, page 327 - 333
反应条件
in toluene
react. with excess t-C4H9NCO in toluene at room temp.;;
参考文献
Gmelin Handbook: Ni: Org.Verb.1, 1.1.6.4.1, page 327 - 333
参考文献
Baker, R.; Cookson, R. C.; Vinson, J. R.
J. Chem. soc. Chem. Comun., 1974 , p. 515 - 516
参考文献
Gmelin Handbook: Ni: Org.Verb.2, 1.5.2.1.3, page 204 - 210
参考文献
Gmelin Handbook: Ni: Org.Verb.2, 1.6.1.2, page 225 - 243
反应条件
water; triphenylphosphine; cesium fluoride; palladium dichloride in dimethyl sulfoxide
T=90°C;
参考文献
Jiang, Huanfeng; Liu, Bifu; Li, Yibiao; Wang, Azhong; Huang, Huawen
Organic Letters, 2011 , vol. 13, # 5 p. 1028 - 1031
反应条件
water; triphenylphosphine; cesium fluoride; palladium dichloride in dimethyl sulfoxide
T=90°C;
参考文献
Jiang, Huanfeng; Liu, Bifu; Li, Yibiao; Wang, Azhong; Huang, Huawen
Organic Letters, 2011 , vol. 13, # 5 p. 1028 - 1031
反应条件
water; sodium acetate in acetonitrile
T=0°C; 1.16667 h; Inert atmosphere;
参考文献
Xia, Zhonghua; Zhu, Qiang
Organic Letters, 2013 , vol. 15, # 16 p. 4110 - 4113
反应条件
water; triphenylphosphine; cesium fluoride; palladium dichloride in dimethyl sulfoxide
T=110°C; 15 h;
参考文献
Jiang, Huanfeng; Liu, Bifu; Li, Yibiao; Wang, Azhong; Huang, Huawen
Organic Letters, 2011 , vol. 13, # 5 p. 1028 - 1031