119072-55-8合成路线 (共 225 条)
反应条件
1: 68 percent / 15 h / Ambient temperature
2: 94 percent / CsF / benzyltriethylammonium chloride / tetrahydrofuran / 1 h / Heating
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参考文献
Sebti, Said; Foucaud, Andre
Synthesis, 1983 , # 7 p. 546 - 549
反应条件
water; triphenylphosphine; cesium fluoride; palladium dichloride in dimethyl sulfoxide
T=90°C;
参考文献
Jiang, Huanfeng; Liu, Bifu; Li, Yibiao; Wang, Azhong; Huang, Huawen
Organic Letters, 2011 , vol. 13, # 5 p. 1028 - 1031
反应条件
tetrakis(triphenylphosphine) palladium(0); water; caesium carbonate in acetonitrile
T=60°C; 10 h; Inert atmosphere;
参考文献
Zhou, Fengtao; Ding, Ke; Cai, Qian
Chemistry - A European Journal, 2011 , vol. 17, # 44 p. 12268 - 12271
反应条件
tetrakis(triphenylphosphine) palladium(0); water; caesium carbonate in acetonitrile
T=60°C; 10 h; Inert atmosphere;
参考文献
Zhou, Fengtao; Ding, Ke; Cai, Qian
Chemistry - A European Journal, 2011 , vol. 17, # 44 p. 12268 - 12271
反应条件
tetrakis(triphenylphosphine) palladium(0); water; caesium carbonate in 1,4-dioxane
10 h; Inert atmosphereReflux;
参考文献
Zhou, Fengtao; Ding, Ke; Cai, Qian
Chemistry - A European Journal, 2011 , vol. 17, # 44 p. 12268 - 12271
反应条件
in tetrahydrofuran
T=20°C; 9 h;
参考文献
Ripka, Amy S.; Diaz, David D.; Sharpless, K. Barry; Finn
Organic Letters, 2003 , vol. 5, # 9 p. 1531 - 1533
反应条件
in tetrahydrofuran
0.333333 h; Ambient temperature;
参考文献
Berree, Fabienne; Malvaut, Yvelise; Marchand, Evelyne; Morel, Georges
Journal of Organic Chemistry, 1993 , vol. 58, # 22 p. 6022 - 6029
反应条件
in tetrahydrofuran
0.166667 h; Ambient temperature;
参考文献
Morel,G.; Marchand,E.
Tetrahedron, 1984 , vol. 40, p. 1075
反应条件
water; triphenylphosphine; cesium fluoride; palladium dichloride in dimethyl sulfoxide
T=90°C;
参考文献
Jiang, Huanfeng; Liu, Bifu; Li, Yibiao; Wang, Azhong; Huang, Huawen
Organic Letters, 2011 , vol. 13, # 5 p. 1028 - 1031
反应条件
titanium tetrachloride in dichloromethane
T=0°C; Yield given. Yields of byproduct given;
参考文献
Ito, Yoshihiko; Kato, Hidehito; Imai, Hiroshi; Saegusa, Takeo
Journal of the American Chemical Society, 1982 , vol. 104, # 23 p. 6449 - 6450