119072-55-8合成路线 (共 225 条)
反应条件
potassium fluoride; 18-crown-6 ether; water in tetrahydrofuran
T=30°C; 16 h; Inert atmosphere;
参考文献
Kaicharla, Trinadh; Thangaraj, Manikandan; Biju, Akkattu T.
Organic Letters, 2014 , vol. 16, # 6 p. 1728 - 1731
反应条件
water; triphenylphosphine; cesium fluoride; palladium dichloride in dimethyl sulfoxide
T=90°C;
参考文献
Jiang, Huanfeng; Liu, Bifu; Li, Yibiao; Wang, Azhong; Huang, Huawen
Organic Letters, 2011 , vol. 13, # 5 p. 1028 - 1031
反应条件
water; triphenylphosphine; cesium fluoride; palladium dichloride in dimethyl sulfoxide
T=110°C; 15 h;
参考文献
Jiang, Huanfeng; Liu, Bifu; Li, Yibiao; Wang, Azhong; Huang, Huawen
Organic Letters, 2011 , vol. 13, # 5 p. 1028 - 1031
反应条件
potassium fluoride; 18-crown-6 ether; water in tetrahydrofuran
T=30°C; 16 h; Inert atmosphere; Overall yield = 61 percent; Overall yield = 0.060 g; regioselective reaction;
参考文献
Kaicharla, Trinadh; Thangaraj, Manikandan; Biju, Akkattu T.
Organic Letters, 2014 , vol. 16, # 6 p. 1728 - 1731
参考文献
Saegusa,T.; Ito,Y.
Synthesis, 1975 , p. 291 - 300
反应条件
sodium tris(acetoxy)borohydride
T=-40 - 20°C;
参考文献
Kiselyov, Alexander S.
Tetrahedron Letters, 2005 , vol. 46, # 26 p. 4487 - 4490
参考文献
Ito,Y. et al.
Synthetic Communications, 1976 , vol. 6, p. 429 - 433
参考文献
Ito,Y. et al.
Journal of Organometallic Chemistry, 1975 , vol. 85, p. 395 - 401
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; caesium carbonate in toluene
16 h; Inert atmosphereReflux;
参考文献
Geden, Joanna V.; Pancholi, Alpa K.; Shipman, Michael
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4158 - 4164
反应条件
titanium tetrachloride in dichloromethane
T=-50 - 20°C;
参考文献
Pellissier, Helene; Meou, Alain; Gil, Gerard
Tetrahedron Letters, 1986 , vol. 27, # 30 p. 3505 - 3506