119072-55-8合成路线 （共 225 条）
反应条件
titanium tetrachloride in dichloromethane
1.) -50 deg C, 2.) 3 h room temperature;
参考文献
Pellissier, Helene; Meou, Alain; Gil, Gerard
Tetrahedron Letters, 1986 , vol. 27, # 26 p. 2979 - 2980
反应条件
titanium tetrachloride in dichloromethane
T=-50 - 20°C; 3 h;
参考文献
Pellissier, Helene; Meou, Alain; Gil, Gerard
Tetrahedron Letters, 1986 , vol. 27, # 30 p. 3505 - 3506
反应条件
titanium tetrachloride in dichloromethane
1.) -50 deg C, 2.) 3 h room temperature;
参考文献
Pellissier, Helene; Meou, Alain; Gil, Gerard
Tetrahedron Letters, 1986 , vol. 27, # 26 p. 2979 - 2980
反应条件
unter Ausschluss von Luft und Licht im Rohr;
参考文献
Kharasch; Kleiger; Mayo
Journal of Organic Chemistry, 1939 , vol. 4, p. 431,434
Full Text Show Details
Kharasch; Hannum
Journal of the American Chemical Society, 1934 , vol. 56, p. 712
反应条件
selenium; triethylamine in tetrahydrofuran
参考文献
Minozzi, Matteo; Nanni, Daniele; Walton, John C.
Journal of Organic Chemistry, 2004 , vol. 69, # 6 p. 2056 - 2069
反应条件
in dichloromethane
1 h; Ambient temperature;
参考文献
Roques; Mazieres; Majoral; Sanchez; Foucaud
Journal of Organic Chemistry, 1989 , vol. 54, # 23 p. 5535 - 5539
反应条件
1: bis(4-methoxyphenyl)methyl chloride With zinc(II) chloride in diethyl ether; dichloromethane
T=-30°C;
2: tert-butylisonitrile in diethyl ether; dichloromethane
T=-30 - 20°C;
3: in diethyl ether; dichloromethane
T=20°C; Further stages.;
参考文献
Tumanov, Vasily V.; Tishkov, Alexander A.; Mayr, Herbert
Angewandte Chemie - International Edition, 2007 , vol. 46, # 19 p. 3563 - 3566
反应条件
1: With Ti(NMe2)2(dpma); cyclohexylamine in toluene
T=100°C; 24 h; Inert atmosphere;
2: With hydroxylamine hydrochloride in ethanol; toluene
T=25°C; 16 h; Inert atmosphere; regioselective reaction;
参考文献
Dissanayake, Amila A.; Odom, Aaron L.
Tetrahedron, 2012 , vol. 68, # 3 p. 807 - 812
反应条件
1,3-bis-(diphenylphosphino)propane; caesium carbonate; palladium dichloride in toluene
16 h; Inert atmosphereReflux;
参考文献
Geden, Joanna V.; Pancholi, Alpa K.; Shipman, Michael
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4158 - 4164
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; caesium carbonate in toluene
16 h; Inert atmosphereReflux;
参考文献
Geden, Joanna V.; Pancholi, Alpa K.; Shipman, Michael
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4158 - 4164
