119072-55-8合成路线 (共 225 条)
参考文献
Menzel, Henning; Horstmann, Sandra; Behrens, Peter; Baernreuther, Petra; Krueger, Ilka; Jahns, Michael
Chemical Communications, 2003 , # 24 p. 2994 - 2995
反应条件
1: in methanol; dichloromethane T=20°C; 2: With N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; 2 h;
参考文献
Azuaje, Jhonny; Coelho, Alberto; Maatougui, Abdelaziz El; Blanco, Jose Manuel; Sotelo, Eddy
ACS Combinatorial Science, 2011 , vol. 13, # 1 p. 89 - 95
反应条件
tetrakis(triphenylphosphine) palladium(0) in neat (no solvent) byproducts: ((CH3)3Si)2; mixt. of 2 equiv of isonitrile, 5 equiv of organosilylstannane and 0.06 equiv of Pd-complex was heated without solvent at 60°C for 3 h under Ar; distd.; elem. anal.;;
参考文献
Ito, Yoshihiko; Bando, Takashi; Matsuura, Takaharu; Ishikawa, Mitsuo
Journal of the Chemical Society, Chemical Communications, 1986 , # 12 p. 980 - 981
反应条件
1: tert-butylisonitrile; phenylacetylene With Ti(NMe2)2(dpma); cyclohexylamine in toluene T=100°C; 24 h; Inert atmosphere; 2: methanimidamide monoacetate in 1,1-dimethylpropan-1-ol T=140°C; 24 h; Inert atmosphere;
参考文献
Tetrahedron, , vol. 66, # 17 p. 3152 - 3158
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Buchwald, Stephen L.; LaMaire, Susan J.
Tetrahedron Letters, 1987 , vol. 28, # 3 p. 295 - 298
反应条件
water; triphenylphosphine; cesium fluoride; palladium dichloride in dimethyl sulfoxide T=90°C; 12 h;
参考文献
Jiang, Huanfeng; Liu, Bifu; Li, Yibiao; Wang, Azhong; Huang, Huawen
Organic Letters, 2011 , vol. 13, # 5 p. 1028 - 1031
反应条件
water; triphenylphosphine; cesium fluoride; palladium dichloride in dimethyl sulfoxide T=90°C;
参考文献
Jiang, Huanfeng; Liu, Bifu; Li, Yibiao; Wang, Azhong; Huang, Huawen
Organic Letters, 2011 , vol. 13, # 5 p. 1028 - 1031
反应条件
potassium fluoride; 18-crown-6 ether; water in tetrahydrofuran T=30°C; 16 h; Inert atmosphere; Reagent/catalyst;
参考文献
Kaicharla, Trinadh; Thangaraj, Manikandan; Biju, Akkattu T.
Organic Letters, 2014 , vol. 16, # 6 p. 1728 - 1731
反应条件
water; triphenylphosphine; cesium fluoride; palladium dichloride in dimethyl sulfoxide T=110°C; 15 h;
参考文献
Jiang, Huanfeng; Liu, Bifu; Li, Yibiao; Wang, Azhong; Huang, Huawen
Organic Letters, 2011 , vol. 13, # 5 p. 1028 - 1031
反应条件
water; caesium carbonate in acetone T=0°C; 0.333333 h; Schlenk techniqueInert atmosphere;
参考文献
Xia, Zhonghua; Zhu, Qiang
Organic Letters, 2013 , vol. 15, # 16 p. 4110 - 4113