119072-55-8合成路线 （共 225 条）
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; caesium carbonate in toluene 16 h; Inert atmosphereReflux;
参考文献
Geden, Joanna V.; Pancholi, Alpa K.; Shipman, Michael
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4158 - 4164
反应条件
1: With C15H24N4Ti in toluene T=100°C; 24 h; Inert atmosphere; 2: With pyridine; hydrazine hydrate T=150°C; 12 h; Inert atmosphere; regioselective reaction;
参考文献
Majumder, Supriyo; Gipson, Kevin R.; Staples, Richard J.; Odom, Aaron L.
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 11-12 p. 2013 - 2023
反应条件
1: With Ti(NMe2)2(dpma) in toluene T=100°C; 24 h; Inert atmosphere; 2: With pyridine; hydrazine hydrate T=150°C; 12 h; Inert atmosphere; regioselective reaction;
参考文献
Majumder, Supriyo; Gipson, Kevin R.; Staples, Richard J.; Odom, Aaron L.
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 11-12 p. 2013 - 2023
反应条件
1: With Ti(NMe2)2(dpma); cyclohexylamine in toluene T=100°C; 24 h; Inert atmosphere; 2: With hydroxylamine hydrochloride in ethanol; toluene T=25°C; 16 h; Inert atmosphere; regioselective reaction;
参考文献
Dissanayake, Amila A.; Odom, Aaron L.
Tetrahedron, 2012 , vol. 68, # 3 p. 807 - 812
参考文献
Saegusa,T.; Ito,Y.
Synthesis, 1975 , p. 291 - 300
反应条件
2,4-di-Nitrobenzene in benzene T=20°C; Addition; 24 h; Irradiation; Further byproducts given. Title compound not separated from byproducts;
参考文献
Leardini, Rino; Nanni, Daniele; Zanardi, Giuseppe
Journal of Organic Chemistry, 2000 , vol. 65, # 9 p. 2763 - 2772
反应条件
Yield given. Multistep reaction;
参考文献
Buchwald, Stephen L.; LaMaire, Susan J.
Tetrahedron Letters, 1987 , vol. 28, # 3 p. 295 - 298
反应条件
triethylamine in methanol
参考文献
LEIBNIZ-INSTITUT FUR PFLANZENBIOCHEMIE; Wessjohann, Ludger A.; Henze, Michael; Kreye, Oliver; Rivera, Daniel Garcia
Patent: US2013/203960 A1, 2013 ;
Location in patent: Page/Page column ;
反应条件
N-(benzoyl)glycine; methanol 24 h;
参考文献
Skorna,G.; Ugi,I.
Chemische Berichte, 1979 , vol. 112, p. 776 - 777
反应条件
in toluene addn. of CNt-Bu to a soln. of the iron complex, stirring at room temp. for 6 h, condensing the volatiles into a flask cooled by liquid nitrogen and containing maleic acid anhydride, refluxing the flask for 3 h; removal of the volatiles in vacuo, mass spectroscopy;
参考文献
Organometallics, , vol. 13, p. 619 - 630
