1: thiophenol With sodium hydride in N,N-dimethyl-formamide
T=20°C; 0.166667 h;
2: 3-methyl-but-2-en-1-yl acetate With tetrakis(triethylphosphite)nickel(O) in tetrahydrofuran; N,N-dimethyl-formamide
20 h; Heating; Further stages.;
lt;Mo(CO)4Br2gt;2 in dichloromethane
1 h; Ambient temperature; Yield given;
参考文献
Malkov, Andrei V.; Davis, Stuart L.; Baxendale, Ian R.; Mitchell, William L.; Kocovsky, Pavel
Journal of Organic Chemistry, 1999 , vol. 64, # 8 p. 2751 - 2764