1: poly(dibutylstannane) With lithium diisopropyl amide in tetrahydrofuran; hexane
T=-45°C; 0.5 h; Cooling with liquid nitrogen/chlorobenzene;
2: benzaldehyde in tetrahydrofuran; hexane
T=-45 - -30°C; Cooling with liquid nitrogen/chlorobenzene;
参考文献
Feldman, Jerald; McLain, Stephan J.; Barsotti, Robert John; O'Neil, James William
Patent: US2007/141386 A1, 2007 ;
Location in patent: Page/Page column 7-8 ;
