tert.-butylhydroperoxide in water; toluene T=-20°C; 12 h;

1,2:4,5-di-O-cyclohexylidene-D-fructopyranose; alpha,alpha-dimethylbenzyl hydroperoxide; VO(O(propyl))3; N-ethyl-N,N-diisopropylamine in water; ethyl acetate T=20 - 55°C; 20.1667 - 20.25 h; Product distribution / selectivity;

1: With methanol T=25°C; 0.5 h; 2: With methanol; sodium hydroxide; water T=25°C; 3.16667 h; 3: With water; acetic acid in methanol pH=6.8;

1: With titanium(IV) isopropylate; diethyl (2S,3S)-tartrate in water T=20 - 70°C; 1.5 h; Heating / reflux; 2: With alpha,alpha-dimethylbenzyl hydroperoxide in water T=20°C; Product distribution / selectivity;

triethylamine in methanol Chiral supercritical fluid chromatographyResolution of racemate; Purification / work up;

enantiomeric resolution; inclusion complexation with (R)-(+)-2,2'-dihydroxy-1,1'-binaphthyl;