1191415-24-3合成路线 （共 12 条）
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=20 - 45°C; 4.16667 h;
参考文献
Ji, Yong; Li, Pinhua; Zhang, Xiuli; Wang, Lei
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 24 p. 4095 - 4101
反应条件
palladium diacetate; potassium carbonate; dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine in tetrahydrofuran T=110°C; P=7757.43 Torr; 15 h; Autoclave;
参考文献
Organic Letters, , vol. 13, # 11 p. 2868 - 2871
反应条件
palladium diacetate; potassium carbonate; dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine in tetrahydrofuran T=110°C; P=7757.43 Torr; 15 h; Autoclave;
参考文献
Organic Letters, , vol. 13, # 11 p. 2868 - 2871
反应条件
1: copper(l) iodide; sodium carbonate / N,N-dimethyl-formamide / 6 h / 80 °C / Inert atmosphere 2: palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 6 h / 120 °C / Inert atmosphere View Scheme
参考文献
Zhou, Wei; Chen, Wei; Wang, Lei
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 21 p. 4172 - 4178
反应条件
palladium diacetate; potassium carbonate; dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine in tetrahydrofuran T=110°C; P=7757.43 Torr; 15 h; Autoclave;
参考文献
Organic Letters, , vol. 13, # 11 p. 2868 - 2871
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium phosphate; triethylamine; palladium dichloride in 1,4-dioxane; water
T=110°C; 16 h; Inert atmosphere;
参考文献
Bryan, Christopher S.; Braunger, Julia A.; Lautens, Mark
Angewandte Chemie, International Edition, 2009 , vol. 48, # 38 p. 7064 - 7068
Angewandte Chemie, 2009 , vol. 121, # 38 p. 7198 - 7202
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium phosphate; triethylamine; palladium dichloride in 1,4-dioxane
T=110°C; 16 h; Inert atmosphere;
参考文献
Bryan, Christopher S.; Braunger, Julia A.; Lautens, Mark
Angewandte Chemie, International Edition, 2009 , vol. 48, # 38 p. 7064 - 7068
Angewandte Chemie, 2009 , vol. 121, # 38 p. 7198 - 7202
反应条件
1: 2-(2,2-dibromovinyl)benzenethiol With tetrabutyl ammonium fluoride in N,N-dimethyl-formamide
T=20°C; 4 h; Sealed tubeInert atmosphere;
2: benzenesulphinic acid sodium salt With copper diacetate; triethylamine; palladium dichloride in N,N-dimethyl-formamide
T=110°C; 12 h; Sealed tubeInert atmosphere;
参考文献
Chen, Wei; Li, Pinhua; Miao, Tao; Meng, Ling-Guo; Wang, Lei
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 3 p. 420 - 424
反应条件
tetrabutyl ammonium fluoride; palladium diacetate; triphenylphosphine in 1-methyl-pyrrolidin-2-one
T=80°C; tandem elimination-addition-Hiyama coupling; 12 h;
参考文献
Liu, Jie; Chen, Wei; Ji, Yong; Wang, Lei
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 8 p. 1585 - 1592
反应条件
1: caesium carbonate; copper(l) iodide / ethanol / 8 h / 80 °C / |Sealed tube; |Green chemistry
2: caesium carbonate; palladium dichloride / ethanol / 8 h / 80 °C / |Green chemistry
View Scheme
参考文献
Ji, Yong; Li, Pinhua; Zhang, Xiuli; Wang, Lei
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 24 p. 4095 - 4101
