2,3-二氢噻吩1,1-二氧化物合成路线 （共 17 条）
反应条件
2,6-dichloro-benzonitrile in tetrahydrofuran 4 h; Ambient temperature;
参考文献
Ren, Xiao-Feng; Turos, Edward; Lake, Charles H.; Churchill, Melvyn Rowen
Journal of Organic Chemistry, 1995 , vol. 60, # 20 p. 6468 - 6483
反应条件
potassium hydroxide in 1,4-dioxane; water 5 h; Heating;
参考文献
Parkhomenko, P. I.; Rybakova, M. V.; Bezmenova, T. E.; Zaika, T. D.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1980 , vol. 16, # 11 p. 1122 - 1124
Khimiya Geterotsiklicheskikh Soedinenii, 1980 , vol. 16, # 11 p. 1482 - 1484
反应条件
hydrogenchloride in water 10 h; Heating;
参考文献
Parkhomenko, P. I.; Rybakova, M. V.; Bezmenova, T. E.; Zaika, T. D.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1980 , vol. 16, # 11 p. 1122 - 1124
Khimiya Geterotsiklicheskikh Soedinenii, 1980 , vol. 16, # 11 p. 1482 - 1484
反应条件
in tetrahydrofuran T=-78°C; 2 h;
参考文献
Chou, Ta-shue; Hung, Su Chun; Tso, Hsi-Hwa
Journal of Organic Chemistry, 1987 , vol. 52, # 15 p. 3394 - 3399
反应条件
sodium hydroxide T=95 - 100°C; 2.5 h;
参考文献
Mukhamedova, L. A.; Kursheva, L. I.; Nechaeva, M. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 4 p. 360 - 361
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , vol. 18, # 4 p. 478 - 479
反应条件
triethylamine in 1,4-dioxane; water 5 h; Heating;
参考文献
Parkhomenko, P. I.; Rybakova, M. V.; Bezmenova, T. E.; Zaika, T. D.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1980 , vol. 16, # 11 p. 1122 - 1124
Khimiya Geterotsiklicheskikh Soedinenii, 1980 , vol. 16, # 11 p. 1482 - 1484
反应条件
sodium carbonate in water 5 h; Heating;
参考文献
Parkhomenko, P. I.; Rybakova, M. V.; Bezmenova, T. E.; Zaika, T. D.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1980 , vol. 16, # 11 p. 1122 - 1124
Khimiya Geterotsiklicheskikh Soedinenii, 1980 , vol. 16, # 11 p. 1482 - 1484
反应条件
potassium in toluene Ambient temperature;
参考文献
Chou, Ta-shue; Chen, Mei-Man
Heterocycles, 1987 , vol. 26, # 11 p. 2829 - 2834
反应条件
sodium hydride Alkylation with various alkyliodides under various circumstances (DMF or DME, with/without AgNO3); Product distributionMechanism;
参考文献
Chou, Ta-shue; Tso, Hsi-Hua; Chang, Lee-Jean
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 515 - 520
反应条件
dihydrogen peroxide; acetic acid
参考文献
Birch; McAllan
Journal of the Chemical Society, 1951 , p. 2556,2561
