3-乙基-2,2-二甲基环氧乙烷合成路线 （共 17 条）
反应条件
3,3-dimethyldioxirane in acetone T=23°C; Kinetics; Further Variations:Solvents;
参考文献
Baumstark; Franklin; Vasquez; Crow
Molecules, 2004 , vol. 9, # 3 p. 117 - 124
反应条件
(2-diethylaminocarbonylpyridine)2VO(O2) in dichloromethane T=20°C; 2 h; further reagents (pyridine-2-carboxylate)VO(O2)(H2O)2, <(pyridine-2-carboxylate)2VO(O2)>-H+*H2O, <(pyridine-2-carboxylate)2VO(O2)>-H+*HMPT, further solvent MeCN;
参考文献
Mimoun; Saussine; Daire; Postel; Fischer; Weiss
Journal of the American Chemical Society, 1983 , vol. 105, # 10 p. 3101 - 3110
反应条件
1: benzene-d6 2: 60 percent Spectr. / CDCl3 / 72 h / 60 °C View Scheme
参考文献
Robinson, Philip L.; Barry, Carey N.; Kelly, Jeffery W.; Evans, Slayton A.
Journal of the American Chemical Society, 1985 , vol. 107, # 18 p. 5210 - 5219
反应条件
chloroform-d1 T=60°C; 72 h;
参考文献
Robinson, Philip L.; Barry, Carey N.; Kelly, Jeffery W.; Evans, Slayton A.
Journal of the American Chemical Society, 1985 , vol. 107, # 18 p. 5210 - 5219
反应条件
disodium hydrogenphosphate; dihydrogen peroxide in chloroform 24 h; Ambient temperature;
参考文献
Stark, Charles J.
Tetrahedron Letters, 1981 , vol. 22, p. 2089 - 2092
反应条件
pyridine-2-carboxylic acid; [Mn(ClO4)2]*6H2O; dihydrogen peroxide; sodium acetate; 1,2-dichloro-benzene in water; acetone T=0 - 20°C;
参考文献
Saisaha, Pattama; Pijper, Dirk; Van Summeren, Ruben P.; Hoen, Rob; Smit, Christian; De Boer, Johannes W.; Hage, Ronald; Alsters, Paul L.; Feringa, Ben L.; Browne, Wesley R.
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 19 p. 4444 - 4450
反应条件
in toluene T=100°C; 24 h;
参考文献
Robinson, Philip L.; Kelly, Jeffery W.; Evans, Slayton A.
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 26, p. 15 - 24
反应条件
oxygen T=45°C; P=759.8 Torr; 95 h; autoxidation; Product distribution;
参考文献
Bilas, W.; Hoebold, W.; Pritzkow, W.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 1 p. 125 - 141
反应条件
lithium aluminium tetrahydride; oxygen multistep reaction: 1) 45 deg C, 101,3 kPa, 95 h; Product distribution;
参考文献
Bilas, W.; Hoebold, W.; Pritzkow, W.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 1 p. 125 - 141
反应条件
perchloric acid in water 5 h; Ambient temperature;
参考文献
Liebigs Annalen der Chemie, , # 4 p. 518 - 532
