反应条件
1: PhI(OAc)2, I2 / cyclohexane / 50 °C / Irradiation
2: 99 percent / H2 / PtO2 / ethyl acetate / 42 h / 23 °C / 2844.3 Torr
3: RuCl3*H2O, NaIO4 / CCl4; acetonitrile; H2O / 23 °C
4: diethyl ether / 0 °C
5: 89 percent / PhNMe3Br3 / tetrahydrofuran / 23 °C
6: 90 percent / Li2CO3, LiBr / dimethylformamide / 1 h / 80 - 130 °C
7: DIBAL-H / toluene / -78 - 0 °C
8: tetrapropylammonium perruthenate, NMO, 4 Angstroem mol. sieves / CH2Cl2 / 23 °C
9: 91 percent / LiHMDS, Me3SiCl / tetrahydrofuran / -78 °C
10: 91 percent / Davis oxaziridine / CHCl3 / 0 - 23 °C
View Scheme
参考文献
Burke, Steven D.; Kort, Michael E.; Strickland, Sharon M.S.; Organ, Helen M.; Silks III, Louis A.
Tetrahedron Letters, 1994 , vol. 35, # 10 p. 1503 - 1506
