hydrogen; palladium 10 on activated carbon in methanol T=20°C; 23 h;

<b>Multi-step reaction with 2 steps<br /> </b>1: trichlorophosphate / N,N-dimethyl-formamide / 1 h / 80 &deg;C<br />2: sodium azide / N,N-dimethyl-formamide / 22 h / 20 &deg;C<br /> <br /> &nbsp;