3-甲基-2,5-二氢噻吩-1,1-二氧化物合成路线 （共 24 条）
参考文献
Chae, Woo-Ki; Baughman, Sharon A.; Engel, Paul S.; Bruch, Manfred; Oezmeral, Cenan; et al.
Journal of the American Chemical Society, 1981 , vol. 103, # 16 p. 4824 - 4833
反应条件
sodium amalgam; phosphoric acid in tetrahydrofuran Ambient temperature;
参考文献
Chou; Sun
Tetrahedron Letters, 1990 , vol. 31, # 7 p. 1035 - 1038
反应条件
vinyl-magnesium bromide in tetrahydrofuran T=-78°C; 2 h;
参考文献
Journal of Organic Chemistry, , vol. 52, # 15 p. 3394 - 3399
反应条件
in tetrahydrofuran T=-78°C; 2 h;
参考文献
Journal of Organic Chemistry, , vol. 52, # 15 p. 3394 - 3399
反应条件
dihydrogen peroxide; acetic acid
参考文献
Journal of the Chemical Society, , p. 3411,3415
反应条件
1: sodium; liquid ammonia; methanol 2: acetic acid; aqueous (?) hydrogen peroxide View Scheme
参考文献
Journal of the Chemical Society, , p. 3411,3415
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 131, p. 289,291
反应条件
1: 75 percent / LiHMDS / tetrahydrofuran; hexamethylphosphoric acid triamide / 0.08 h / -78 °C 2: 1.) SOCl2; 2.) NaHCO3 / 1.) pyridine; 2.) CDCl3, 125 deg C, 30 min View Scheme
参考文献
Yamada, Sachiko; Suzuki, Hiromasa; Naito, Hiroyuki; Nomoto, Takashi; Takayama, Hiroaki
Journal of the Chemical Society, Chemical Communications, 1987 , # 5 p. 332 - 333
反应条件
1: 1.) BuLi 2: 83 percent / xylene / Heating View Scheme
参考文献
Spicer, Julie A.; Brimble, Margaret A.; Rowan, Daryl D.
Australian Journal of Chemistry, 1993 , vol. 46, # 12 p. 1929 - 1940
反应条件
sulfuric acid; ammonia; lithium 1.) - 65 deg C, 2.) -5 to 0 deg C -> 25 deg C ( 30 min), 40 deg C (20 min); Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Zaks, I. M.; Polunin, E. V.; Moiseenkov, A. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 12 p. 2564 - 2566
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 12 p. 2799 - 2800
