3-甲基-2-环己烯-1-酮合成路线 （共 314 条）
反应条件
pyridine; iodine; bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane 4 h; Ambient temperature;
参考文献
Benhida, Rachid; Blanchard, Pierre; Fourrey, Jean-Louis
Tetrahedron Letters, 1998 , vol. 39, # 38 p. 6849 - 6852
反应条件
iodine in pyridine; dichloromethane
参考文献
Allergan
Patent: US5760276 A1, 1998 ;
US 5760276 A
反应条件
dipyridinium dichromate; iodine in dichloromethane Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Bovonsombat, Pakorn; Angara, Geetha J.; Mc Nelis, Edward
Tetrahedron Letters, 1994 , vol. 35, # 37 p. 6787 - 6790
反应条件
LiN(Cy)2 in diethyl ether T=-78°C; 1 h;
参考文献
Hellou, Jocelyne; Kingston, John F.; Fallis, Alex G.
Synthesis, 1984 , # 12 p. 1014 - 1017
反应条件
1: 3-methyl-cyclohex-2-en-1-one With lithium diisopropyl amide in tetrahydrofuran T=-78°C; 1 h; Inert atmosphere; 2: carbonic acid diethyl ester in tetrahydrofuran T=-78°C; 1 h;
参考文献
Cui, Li-Qian; Dong, Zhi-Lei; Liu, Kai; Zhang, Chi
Organic Letters, 2011 , vol. 13, # 24 p. 6488 - 6491
反应条件
1: 3-methyl-cyclohex-2-en-1-one With lithium diisopropyl amide in tetrahydrofuran; N,N'-dimethyl-N,N'-propyleneurea T=-78°C; 2: [(Cyanocarbonyl)oxy]ethane in tetrahydrofuran; N,N'-dimethyl-N,N'-propyleneurea
参考文献
Cuthbertson, James D.; Godfrey, Andrew A.; Taylor, Richard J. K.
Synlett, 2010 , # 18 p. 2805 - 2807
反应条件
1: copper(I)iodide 2: 40 percent / TiCl4, Ti(O(i)Pr)4 / CH2Cl2 / 1 h / -78 °C 3: 86 percent / tetrahydrofuran / 48 h / Ambient temperature 4: 77 percent / 2N HCl / tetrahydrofuran / 24 h / Ambient temperature View Scheme
参考文献
Takazawa, Osamu; Tamura, Hiroshi; Kogami, Kunio; Hayashi, Kazuo
Chemistry Letters, 1980 , p. 1257 - 1258
反应条件
hydrogenchloride; mercury; zinc
参考文献
Sato, Tadashi; Watanabe, Masami; Watanabe, Toshiyuki; Onoda, Yasuo; Murayama, Eigoro
Journal of Organic Chemistry, 1988 , vol. 53, # 9 p. 1894 - 1899
反应条件
sodium hydroxide; dihydrogen peroxide; 1-(n-butyl)-3-methylimidazolium triflate in water T=25°C; 0.0833333 h;
参考文献
Bortolini, Olga; Campestrini, Sandro; Conte, Valeria; Fantin, Giancarlo; Fogagnolo, Marco; Maietti, Silvia
European Journal of Organic Chemistry, 2003 , # 24 p. 4804 - 4809
反应条件
dihydrogen peroxide in water; acetonitrile T=69.84°C; 5 h;
参考文献
Tang, Bo; Dai, Weili; Sun, Xiaoming; Guan, Naijia; Li, Landong; Hunger, Michael
Green Chemistry, 2014 , vol. 16, # 4 p. 2281 - 2291
