3-甲基-2-环己烯-1-酮合成路线 (共 314 条)
反应条件
in acetonitrile Irradiation; Rate constantQuantum yield;
参考文献
Schuster, David I.; Heibel, George E.; Woning, Jan
Angewandte Chemie, 1991 , vol. 103, # 10 p. 1381 - 1383
反应条件
in acetonitrile Irradiation; Rate constantQuantum yield;
参考文献
Schuster, David I.; Heibel, George E.; Woning, Jan
Angewandte Chemie, 1991 , vol. 103, # 10 p. 1381 - 1383
反应条件
1: 1) DME 2: 96 percent 3: 75 percent / (bipyH2)-CrOCl5 / 8 h / 40 °C / pyridinium chlorochromate, 40 degC, 48 h is also possible 4: 1) LDA/C6H5SeSeC6H5, 2) H2O2 View Scheme
参考文献
Chakraborty, T.K.; Chandrasekaran, S.
Tetrahedron Letters, 1984 , vol. 25, # 27 p. 2895 - 2896
反应条件
sodium hydride in dimethyl sulfoxide 4 h; Ambient temperature;
参考文献
Kirschberg, Thorsten; Mattay, Jochen
Journal of Organic Chemistry, 1996 , vol. 61, # 25 p. 8885 - 8896
反应条件
sodium hydride 1) DMSO, RT, 30 min; 2) DMSO, RT, 1.5 h; Yield given. Multistep reaction;
参考文献
Shibuya, Hirotaka; Tsujii, Shinji; Yamamoto, Yoshio; Miura, Hiromi; Kitagawa, Isao
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 9 p. 3417 - 3427
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tsuda, Tetsuo; Satomi, Hiroshi; Hayashi, Toshio; Saegusa, Takeo
Journal of Organic Chemistry, 1987 , vol. 52, # 3 p. 439 - 443
反应条件
potassium hydroxide; hydrogen; RuCl2lt;(R)-binapgt;(dmf)n*(R,R)-1,2-diphenylethylenediamine in isopropyl alcohol T=28°C; P=6080 Torr; 18 h;
参考文献
Ohkuma, Takeshi; Ikehira, Hideyuki; Ikariya, Takao; Noyori, Ryoji
Synlett, 1997 , # SPEC. ISS. p. 467 - 468
反应条件
lithium aluminium tetrahydride; 4,7,13,18-tetraoxa-1,10-diazabicyclo[8.5.5]eicosane in tetrahydrofuran 0.25 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Loupy, Andre; Seyden-Penne, Jacqueline
Tetrahedron, 1980 , vol. 36, p. 1937 - 1942
反应条件
sodium tetrahydroborate in various solvent(s) T=20°C; 3 h;
参考文献
Synthetic Communications, , vol. 35, # 6 p. 867 - 872
反应条件
sodium tetrahydroborate; non ionic glycosidic surfactant in water 12 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 37, # 1 p. 53 - 56