3-甲基-2-环己烯-1-酮合成路线 （共 314 条）
反应条件
potassium tri-sec-butyl-borohydride in tetrahydrofuran T=0°C; 1 h;
参考文献
Synthetic Communications, , vol. 18, # 1 p. 89 - 96
反应条件
in pentane T=25°C; 1 h; ether; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Giacomelli, Giampaolo; Caporuso, Anna Maria; Lardicci, Luciano
Tetrahedron Letters, 1981 , vol. 22, # 37 p. 3663 - 3666
反应条件
sodium tetrahydroborate in methanol Luche reduction;
参考文献
Schmidt, Valerie A.; Alexanian, Erik J.
Angewandte Chemie - International Edition, 2010 , vol. 49, # 26 p. 4491 - 4494
反应条件
sodium tetrahydroborate; alpha-cyclodextrin in water influence of other cyclodextrin on the reduction; Product distribution;
参考文献
Chenevert, Robert; Chamberland, Daniel
Chemistry Letters, 1985 , p. 1117 - 1118
反应条件
in acetonitrile T=20°C; Mannich reaction;
参考文献
Porzelle, Achim; Williams, Craig M.
Synthesis, 2006 , # 18 p. 3025 - 3030
反应条件
1: 1) DME 2: 96 percent 3: 75 percent / (bipyH2)-CrOCl5 / 8 h / 40 °C / pyridinium chlorochromate, 40 degC, 48 h is also possible 4: 1) LDA/C6H5SeSeC6H5, 2) H2O2 View Scheme
参考文献
Chakraborty, T.K.; Chandrasekaran, S.
Tetrahedron Letters, 1984 , vol. 25, # 27 p. 2895 - 2896
反应条件
1: H2O2; NaOH / ethanol / 0 - 20 °C
2: BF3-Et2O / CH2Cl2 / 0 °C
3: 52 percent / LiAlH(O-tBu)3 / diethyl ether / -78 °C
View Scheme
参考文献
Guerrab, Zineb; Daou, Boujemaa; Fkih-Tetouani, Souad; Ahmar, Mohammed; Cazes, Bernard
Tetrahedron Letters, 2003 , vol. 44, # 30 p. 5727 - 5730
反应条件
sodium tetrahydroborate; cerium(III) chloride in isopropyl alcohol
3 h; Heating;
参考文献
Uzarewicz, A.; Dresler, R.
Polish Journal of Chemistry, 1995 , vol. 69, # 12 p. 1655 - 1658
反应条件
sodium tetrahydroborate; cerium(III) chloride
0.5 h; Heating;
参考文献
Uzarewicz, A.; Dresler, R.
Polish Journal of Chemistry, 1995 , vol. 69, # 12 p. 1655 - 1658
反应条件
sodium tetrahydroborate; cerium(III) chloride
0.5 h; Heating;
参考文献
Uzarewicz, A.; Dresler, R.
Polish Journal of Chemistry, 1995 , vol. 69, # 12 p. 1655 - 1658
