3-甲基-2-环己烯-1-酮合成路线 (共 314 条)
反应条件
sodium tetrahydroborate; cerium(III) chloride
0.5 h; Heating;
参考文献
Uzarewicz, A.; Dresler, R.
Polish Journal of Chemistry, 1995 , vol. 69, # 12 p. 1655 - 1658
反应条件
sodium tetrahydroborate; cerium(III) chloride in isopropyl alcohol
3 h; Heating;
参考文献
Uzarewicz, A.; Dresler, R.
Polish Journal of Chemistry, 1995 , vol. 69, # 12 p. 1655 - 1658
反应条件
sodium tetrahydroborate; cerium(III) chloride
0.5 h; Heating;
参考文献
Uzarewicz, A.; Dresler, R.
Polish Journal of Chemistry, 1995 , vol. 69, # 12 p. 1655 - 1658
反应条件
sodium tetrahydroborate; cerium(III) chloride
0.5 h; Heating;
参考文献
Uzarewicz, A.; Dresler, R.
Polish Journal of Chemistry, 1995 , vol. 69, # 12 p. 1655 - 1658
反应条件
sodium tetrahydroborate; cerium(III) chloride
0.5 h; Heating;
参考文献
Uzarewicz, A.; Dresler, R.
Polish Journal of Chemistry, 1995 , vol. 69, # 12 p. 1655 - 1658
反应条件
(i) TsNHNH2, TsOH, THF, (ii) MeLi, benzene, Et2O; Multistep reaction;
参考文献
Eilbracht, Peter; Jelitte, Ruediger; Trabold, Peter
Chemische Berichte, 1986 , vol. 119, # 1 p. 169 - 181
反应条件
1: 1.) 5percent MeLi / 1.) HMPT, ether, 0 deg C, 15 min, 2.) HMPT, ether, THF, -78 deg C, 15 min
2: 95 percent / lithium diisopropylamide / tetrahydrofuran
3: 1.)lithium diisopropylamide / 1.) -78 deg C
4: 2.) AlCl3
5: 78 percent / KF, H2O2
6: 70 percent / O2 / CH2Cl2 / 10 h / Irradiation
View Scheme
参考文献
Krohn, Karsten; Khanbabaee, Karamali
Angewandte Chemie, 1994 , vol. 106, # 1 p. 100 - 102
反应条件
1: K2CO3 / benzyltriethylammonium chloride / benzene
2: aq. KMnO4, KOH, MgSO4 / methanol / 1.) r.t., 2. ) reflux
3: 30 percent Chromat. / Zn<Hg>, aq. HCl / 1.5 h / Heating
View Scheme
参考文献
Bailey, Karen E.; Davis, Brian R.
Australian Journal of Chemistry, 1995 , vol. 48, # 11 p. 1827 - 1834
反应条件
copper(l) iodide; lithium chloride in tetrahydrofuran
T=-40°C; 0.5 h;
参考文献
Reetz, Manfred T.; Kindler, Alois
Journal of Organometallic Chemistry, 1995 , vol. 502, # 1-2 p. C5 - C7
反应条件
in tetrahydrofuran
T=-70°C; 0.0833333 h;
参考文献
Matsuzawa, Satoshi; Horiguchi, Yoshiaki; Nakamura, Eiichi; Kuwajima, Isao
Tetrahedron, 1989 , vol. 45, # 2 p. 349 - 362