3-甲基-2-环己烯-1-酮合成路线 （共 314 条）
反应条件
potassium hydroxide
1.) 95percent EtOH, reflux, 3 h, 2.) H2O, reflux, 36 h; Yield given. Multistep reaction;
参考文献
Chakraborti, Asit K.; Ray, Jayanta K.; Kundu, Kalyan K.; Chakrabarty, Sephali; Mukherjee, Debabrata; Ghatak, Usha Ranjan
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 2 p. 261 - 273
参考文献
Tanyeli, Cihangir; Demir, Ayhan S.; Dikici, Emre
Tetrahedron Asymmetry, 1996 , vol. 7, # 8 p. 2399 - 2402
反应条件
in benzene
T=80°C; 19 h;
参考文献
Dunlap, Norma K.; Sabol, Mark R.; Watt, David S.
Tetrahedron Letters, 1984 , vol. 25, # 51 p. 5839 - 5842
反应条件
in benzene
T=90°C; 96 h;
参考文献
Sesenoglu, Oezge; Candela Lena, Jose I.; Altinel, Ertan; Birlirakis, Nicolas; Arseniyadis, Simeon
Tetrahedron Asymmetry, 2005 , vol. 16, # 5 p. 995 - 1015
反应条件
1.1: 43 percent / I2 / pyridine; CH2Cl2 / 1 h
2.1: Zn; 1,2-dibromoethane / tetrahydrofuran / 3 h / 0 °C
2.2: 72 percent Spectr. / Pd(PPh3)2Cl2 / tetrahydrofuran; dimethylformamide / 2 h / 23 °C
View Scheme
参考文献
Negishi, Ei-Ichi; Tan, Ze; Liou, Show-Yee; Liao, Baiqiao
Tetrahedron, 2000 , vol. 56, # 52 p. 10197 - 10207
反应条件
copper(l) iodide
1) hexane, diisopropyl ether, -25 deg C, 0.5 h, 2) - 25 deg C, 1 h, 3) 1 h, RT; Yield given. Multistep reaction;
参考文献
Bernasconi, Silvana; Jommi, Giancarlo; Montanari, Stefania; Sisti, Massimo
Gazzetta Chimica Italiana, 1987 , vol. 117, # 2 p. 125 - 128
反应条件
(i), (ii) /BRN= 385737/; Multistep reaction;
参考文献
Stotter,P.L.; Hill,K.A.
Journal of Organic Chemistry, 1973 , vol. 38, # 14 p. 2576 - 2578
反应条件
(i) CuBr*Me2S, (ii) /BRN= 1560601/, (iii) /BRN= 385737/; Multistep reaction;
参考文献
House,H.O.; Wilkins,J.M.
Journal of Organic Chemistry, 1976 , vol. 41, # 25 p. 4031 - 4033
参考文献
Duerr,H. et al.
Chemische Berichte, 1965 , vol. 98, p. 1858 - 1878
反应条件
(i) CuI, Et2O, (ii) /BRN= 605303/, 1,2-dimethoxy-ethane; Multistep reaction;
参考文献
Naef,F.; Decorzant,R.
Helvetica Chimica Acta, 1974 , vol. 57, p. 1317 - 1327
