3-甲基-2-环己烯-1-酮合成路线 (共 314 条)
反应条件
1: 1 M aq. LiOH / CHCl3 / 2 h / Ambient temperature 2: 85 percent / Li, LiOAc, AcOH / 0.25 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 53, # 5 p. 1110 - 1112
反应条件
1: 1.) n-BuLi / 1.) THF, -78 deg C, 30 min, 2.) a) -78 deg C, 2 h, b) RT, 1 h 2: 85 percent / H2O/HgCl2/HgO / methanol / 3 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 15 p. 2825 - 2832
反应条件
3-[{2-[4-(4-{2-[bis-(2-methoxycarbonyl-ethyl)-amino]-ethylcarbamoyl}-phenyldisulfanyl)-benzoylamino]-ethyl}-(2-methoxycarbonyl-ethyl)-amino]-propionic acid methyl ester in benzene T=20°C; 2.5 h; UV-irradiation;
参考文献
Heteroatom Chemistry, , vol. 20, # 1 p. 1 - 11
反应条件
1,2-benzenedicarboxylic acid in water Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 52, # 8 p. 1505 - 1511
反应条件
iron (III) acetylacetonate; oxygen; silica gel in diethyl ether T=20°C; 3 h; Irradiation; Title compound not separated from byproducts;
参考文献
Synthetic Communications, , vol. 31, # 3 p. 349 - 357
反应条件
1: 1.) NaBH4, 2.) AcOH / 1.) EtOH, room temp., 2.) EtOH, room temp., 6 h 2: 60 percent / tetrahydrofuran View Scheme
参考文献
Tetrahedron, , vol. 53, # 22 p. 7445 - 7460
反应条件
3,3-dimethyldioxirane in acetone Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 61, # 5 p. 1830 - 1841
反应条件
3,3-dimethyldioxirane in acetone Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 61, # 5 p. 1830 - 1841
反应条件
in tetrahydrofuran Yields of byproduct given;
参考文献
Comasseto, Joao V.; Lo, Wai L.; Petragnani, Nicola
Tetrahedron, 1997 , vol. 53, # 22 p. 7445 - 7460
反应条件
tert.-butylhydroperoxide; dimethyl(n-butyl)amine; zeolite 4 A; titanium silicalite in toluene T=59.85°C; Epoxidation; 0.25 h; Product distribution; Further Variations:Reagentstime;
参考文献
Journal of Catalysis, , vol. 187, # 1 p. 191 - 201