2-甲基-1,3-环己二酮合成路线 （共 134 条）
参考文献
Wieland; Miescher
Helvetica Chimica Acta, 1950 , vol. 33, p. 2215,2224
参考文献
Wieland; Miescher
Helvetica Chimica Acta, 1950 , vol. 33, p. 2215,2224
反应条件
calcined Mg-Al hydrotalcite in methanol
T=20°C; Michael addition; 24 h; Product distribution; Further Variations:Catalysts;
参考文献
Prescott, Hillary A.; Li, Zhi-Jian; Kemnitz, Erhard; Trunschke, Annette; Deutsch, Jens; Lieske, Heiner; Auroux, Aline
Journal of Catalysis, 2005 , vol. 234, # 1 p. 119 - 130
反应条件
(S)-(-)-2-(diphenylmethyl)pyrrolidine
Addition; Product distribution; Further Variations:Reagents;
参考文献
Bui; Barbas III
Tetrahedron Letters, 2000 , vol. 41, # 36 p. 6951 - 6954
反应条件
in benzene
5 h; Heating;
参考文献
Ishikawa; Uedo; Tani; Saito
Journal of Organic Chemistry, 2001 , vol. 66, # 1 p. 186 - 191
反应条件
triethylamine; dibromotriphenyl-phosphorane in benzene
4 h; Ambient temperature;
参考文献
Piers, Edward; Grierson, John R.; Lau, Cheuk Kun; Nagakura, Isao
Canadian Journal of Chemistry, 1982 , vol. 60, p. 210 - 223
反应条件
iodine; triethylamine; triphenylphosphine in acetonitrile
10 h; Reflux;
参考文献
Tietze, Lutz F.; Vock, Carsten A.; Krimmelbein, Ilsa K.; Wiegand, J. Matthias; Nacke, Linda; Ramachandar, Tokala; Islam, Kazi M. D.; Gatz, Christiane
Chemistry - A European Journal, 2008 , vol. 14, # 12 p. 3670 - 3679
反应条件
1.1: LDA; DMPU / tetrahydrofuran / 2 h / -78 °C
1.2: 65 percent / tetrahydrofuran / 9 h / 0 °C
2.1: 45 percent / Fe(acac)3; NMP / tetrahydrofuran / -30 °C
View Scheme
参考文献
Shawe, Thomas T.; Hansen, Darren B.; Peet, Kelly Ann; Prokopowicz, Anthony S.; Robinson, Patrice M.; Cannon, Annatina; Dougherty, Kathleen E.; Ross, Andrew A.; Landino, Linda M.
Tetrahedron, 1997 , vol. 53, # 5 p. 1547 - 1556
反应条件
triethylamine in ethyl acetate
T=70°C; 10 h; Inert atmosphere;
参考文献
Ling, Taotao; Xu, Jing; Smith, Ryan; Ali, Abbas; Cantrell, Charles L.; Theodorakis, Emmanuel A.
Tetrahedron, 2011 , vol. 67, # 17 p. 3023 - 3029
反应条件
triethylamine in ethyl acetate
12 h; Reflux;
参考文献
Lanfranchi, Don Antoine; Baldovini, Nicolas; Hanquet, Gilles
Synthesis, 2008 , # 23 art. no. Z12008SS, p. 3775 - 3778
