5-甲基-2-乙酰基呋喃合成路线 (共 43 条)
反应条件
N,N'-diacetylpiperazine hydrogen tribromide in methanol T=40°C;
参考文献
Burakov; Kanibolotskii; Osichenko; Mikhailov; Savelova; Kosmynin
Russian Journal of Organic Chemistry, 2001 , vol. 37, # 9 p. 1210 - 1219
反应条件
N-bromosuccinmide in tetrachloromethane Bromination; 5 h; Heating; Product distribution; Further Variations:SolventsCatalystsTemperaturesReagents;
参考文献
Saldabol; Popelis; Shatz; Slavinskaya
Chemistry of Heterocyclic Compounds, 1999 , vol. 35, # 2 p. 161 - 163
反应条件
in water 3 h; Heating;
参考文献
Terenin, V. I.; Kabanova, E. V.; Bundel', Yu. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1991 , vol. 27, # 6 p. 597 - 600
Khimiya Geterotsiklicheskikh Soedinenii, 1991 , vol. 27, # 6 p. 763 - 766
反应条件
sodium tetrahydroborate in ethanol Inert atmosphere;
参考文献
Stepanenko, Viatcheslav; De Jesus, Melvin; Correa, Wildeliz; Bermudez, Lorianne; Vazquez, Cindybeth; Guzman, Irisbel; Ortiz-Marciales, Margarita
Tetrahedron Asymmetry, 2009 , vol. 20, # 23 p. 2659 - 2665
反应条件
alkaline aqueous alkali hypochlorite solution
参考文献
Farrar; Levine
Journal of the American Chemical Society, 1950 , vol. 72, p. 3695,3696, 3697
反应条件
potassium hydroxide in isopropyl alcohol 24 h; Ambient temperature;
参考文献
Kuz'min, V. I.; Losev, A. S.; Morozov, I. S.; Pavlova, E. P.; Samoilov, N. N.; et al.
Pharmaceutical Chemistry Journal, 1993 , vol. 27, # 8 p. 555 - 561
Khimiko-Farmatsevticheskii Zhurnal, 1993 , vol. 27, # 8 p. 19 - 24
反应条件
sodium hydroxide in ethanol Claisen-Schmidt Condensation; Reflux;
参考文献
Lam, Kok Wai; Lajis, Nordin H.; Uddin, Reaz; Ul-Haq, Zaheer; Liew, Choi Yi; Tham, Chau Ling; Israf, Daud A.; Syahida, Ahmad; Rahman, Mohd. Basyaruddin Abdul
Medicinal Chemistry Research, 2012 , vol. 21, # 8 p. 1953 - 1966,14
反应条件
potassium hydroxide; hydrazine hydrate in water; ethylene glycol
2 h; Heating;
参考文献
Baig, Mirza Azam; Banthorpe, Derek V.; Carr, Graham; Whittaker, David
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 1981 - 1986
反应条件
nickel; CdO
T=250°C; Hydrogenation;
参考文献
Schuikin; Bel'skii
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 1096,1099; engl. Ausg. S. 1066
反应条件
1: diethyl ether
2: potassium acetate; nitrogen
3: palladium/strontium carbonate; diethyl ether / Hydrogenation
View Scheme
参考文献
Fetizon; Baranger
Bulletin de la Societe Chimique de France, 1957 , p. 1311,1315