5-甲基-2-乙酰基呋喃合成路线 （共 43 条）
反应条件
magnesium
1) ether; 2) ether, 20 min, reflux; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Weyerstahl, Peter; Brendel, Joachim
Liebigs Annalen der Chemie, 1988 , p. 1015 - 1016
反应条件
magnesium
1) ether; 2) ether, 30 min, reflux; 2 d, stirring; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Weyerstahl, Peter; Brendel, Joachim
Liebigs Annalen der Chemie, 1988 , p. 1015 - 1016
反应条件
N-bromosuccinmide in tetrachloromethane
0.5 h; Heating;
参考文献
Mehner, Alexander; Montero, Ana L.; Martinez, Ricardo; Spange, Stefan
Molecules, 2007 , vol. 12, # 3 p. 634 - 640
反应条件
N-bromosuccinmide in tetrachloromethane
Bromination; 5 h; Heating; Product distribution; Further Variations:SolventsCatalystsTemperaturesReagents;
参考文献
Saldabol; Popelis; Shatz; Slavinskaya
Chemistry of Heterocyclic Compounds, 1999 , vol. 35, # 2 p. 161 - 163
反应条件
1: 76 percent / potassium hydroxide, hydrazine hydrate / ethane-1,2-diol; H2O / 2 h / Heating
2: 68 percent / conc. H2SO4 / acetic acid; H2O / 5 h / Heating
View Scheme
参考文献
Baig, Mirza Azam; Banthorpe, Derek V.; Carr, Graham; Whittaker, David
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 1981 - 1986
反应条件
hydrogen; platinum
T=200°C;
参考文献
Shuikin,N.I. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1961 , p. 334 - 335
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1961 , p. 363 - 364
参考文献
Fetizon; Baranger
Bulletin de la Societe Chimique de France, 1957 , p. 1311,1315
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Farrar; Levine
Journal of the American Chemical Society, 1950 , vol. 72, p. 3695,3696, 3697
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Reichstein
Helvetica Chimica Acta, 1930 , vol. 13, p. 349,353
反应条件
1: ammonium polysulfide; dioxane / 110 °C
2: aqueous KOH-solution
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参考文献
Blanchette; Brown
Journal of the American Chemical Society, 1952 , vol. 74, p. 2098
反应条件
triethylamine in N,N-dimethyl-formamide
T=60°C; 16 h;
参考文献
Komarov, N. V.; Lisovin, E. G.; Komarov, A. N.; Chekhun, A. L.; Kul'nevich, V. G.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 8 p. 1862 - 1865,1651 - 1653
反应条件
1: N-bromosuccinimide; AIBN / CCl4 / 1 h / Heating
2: acetic acid / 2 h / Heating
3: KOH / 1 h / Heating
View Scheme
参考文献
Mehner, Alexander; Montero, Ana L.; Martinez, Ricardo; Spange, Stefan
Molecules, 2007 , vol. 12, # 3 p. 634 - 640
