2-(2-甲氧基乙基)-苯甲醇合成路线 （共 3 条）
参考文献
Cremeens, Matthew E.; Hughes, Thomas S.; Carpenter, Barry K.
Journal of the American Chemical Society, 2005 , vol. 127, # 18 p. 6652 - 6661
反应条件
1: 92 percent / PCC 2: 61 percent / ethanol / 1.) 60 deg C, 3 h, 2.) room temp., 3 h, 3.) -20 deg C, overnight 3: sodium hydride / 1.) THF, 2 h, 2.) pentane, 2 h 4: 60 °C / 0 Torr 5: 8.9 percent / p-toluenesulfonic acid / ethanol View Scheme
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1465 - 1473
反应条件
1: 92 percent / PCC
2: 61 percent / ethanol / 1.) 60 deg C, 3 h, 2.) room temp., 3 h, 3.) -20 deg C, overnight
3: sodium hydride / 1.) THF, 2 h, 2.) pentane, 2 h
4: 60 °C / 0 Torr
5: 8.9 percent / p-toluenesulfonic acid / ethanol
6: bromine / benzene / Irradiation
View Scheme
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1465 - 1473
