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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
119367-74-7
合成路线
（共 10 条）
119367-74-7
→
反应条件
493-05-0
异色满
反应条件
1: sodium hydride / 1.) THF, 2 h, 2.) pentane, 2 h 2: 60 °C / 0 Torr 3: 8.9 percent / p-toluenesulfonic acid / ethanol View Scheme
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1465 - 1473
119367-74-7
→
反应条件
493-05-0
异色满
+
26164-06-7
+
81887-53-8
+
15018-15-2
反应条件
sodium methylate in methanol 2 h; Ambient temperatureIrradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1465 - 1473
119367-74-7
→
反应条件
493-05-0
异色满
+
5368-66-1
+
81887-53-8
+
15018-15-2
反应条件
sodium methylate in methanol 2 h; Ambient temperatureIrradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1465 - 1473
119367-74-7
→
反应条件
493-05-0
异色满
+
81887-53-8
+
15018-15-2
+
119367-76-9
反应条件
sodium methylate in methanol 2 h; Ambient temperatureIrradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1465 - 1473
119367-74-7
→
反应条件
493-05-0
异色满
+
81887-53-8
+
15018-15-2
+
119367-77-0
反应条件
sodium methylate in methanol 2 h; Ambient temperatureIrradiation; Yield given. Yields of byproduct given;
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1465 - 1473
67-56-1
甲醇
+
119367-74-7
→
反应条件
493-05-0
异色满
+
81887-53-8
+
15018-15-2
+
119367-76-9
反应条件
in methanol 2 h; Ambient temperatureIrradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1465 - 1473
119367-74-7
→
反应条件
493-05-0
异色满
+
81887-53-8
+
119367-76-9
+
119367-77-0
反应条件
sodium methylate in methanol 2 h; Ambient temperatureIrradiation; Product distributionMechanism;
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1465 - 1473
119367-74-7
→
反应条件
493-05-0
异色满
+
26164-06-7
+
81887-53-8
+
15018-15-2
反应条件
sodium methylate in methanol 2 h; Ambient temperatureIrradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1465 - 1473
119367-74-7
→
反应条件
50683-32-4
反应条件
1: sodium hydride / 1.) THF, 2 h, 2.) pentane, 2 h 2: 60 °C / 0 Torr 3: 8.9 percent / p-toluenesulfonic acid / ethanol 4: bromine / benzene / Irradiation View Scheme
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1465 - 1473
119367-74-7
→
反应条件
493-05-0
异色满
+
5368-66-1
+
81887-53-8
+
15018-15-2
反应条件
sodium methylate in methanol 2 h; Ambient temperatureIrradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1465 - 1473
