T=280°C; P=0.001 Torr; Yield given. Further byproducts given. Yields of byproduct given;

T=280°C; P=0.001 Torr; Yield given. Further byproducts given. Yields of byproduct given;

T=280°C; P=0.001 Torr; Yield given. Further byproducts given. Yields of byproduct given;

T=280°C; P=0.001 Torr; Product distributionMechanism;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '4122952', constants.ctx, '0')">sodium hydride</a> <br />&nbsp;1.) THF, 2 h, 2.) pentane, 2 h;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 3 steps<br /> </b>1: 63 percent / PCC<br />2: 79 percent / 1.) 60 deg C, 3 h, 2.) room temp., 3 h, 3.) -20 deg C, overnight<br />3: sodium hydride / 1.) THF, 2 h, 2.) pentane, 2 h<br /> <br /> &nbsp;

<b>Multi-step reaction with 6 steps<br /> </b>2: 68 percent / sodium hydroxide / aq. ethanol / 10 h / Heating<br />3: 80 percent / lithium aluminum hydride / diethyl ether / 1 h / Heating<br />4: 63 percent / PCC<br />5: 79 percent / 1.) 60 deg C, 3 h, 2.) room temp., 3 h, 3.) -20 deg C, overnight<br />6: sodium hydride / 1.) THF, 2 h, 2.) pentane, 2 h<br /> <br /> &nbsp;