bis(η4-1,5-cyclooctadiene)-di-μ-methoxy-diiridium(I); 4,4'-di-tert-butyl-2,2'-dipyridyl in tetrahydrofuran T=25°C; 8 h; Title compound not separated from byproducts;
参考文献
Chotana, Ghayoor A.; Rak, Michael A.; Smith, Milton R.
Journal of the American Chemical Society, 2005 , vol. 127, # 30 p. 10539 - 10544
Terpinski, Jacek; Denney, Dorothy Z.; Beveridge, Richard; Cox, Phillip D.; Moss, Robert A.
Magnetic Resonance in Chemistry, 1987 , vol. 25, p. 923 - 927
1: With diisobutylaluminium hydride in toluene T=0°C; 0.00555556 h; Flow reactor; 2: With water; tartaric acid disodium salt in toluene T=0°C; chemoselective reaction;
参考文献
Munoz, Juan De M.; Alcazar, Jesus; De La Antonio, Hoz; Diaz-Ortiz, Angel
Tetrahedron Letters, 2011 , vol. 52, # 46 p. 6058 - 6060
1: anhydrous 1-octyne With n-butyllithium in tetrahydrofuran; hexane T=0°C; 2: With zinc dibromide in tetrahydrofuran; hexane T=0°C; 3: 4-fluorobenzenecarbonitrile With n-tridecane; [NiCl2(PMe3)2] in tetrahydrofuran T=65°C; 45 h; Further stages.;
参考文献
Penney, Jonathan M.; Miller, Joseph A.
Tetrahedron Letters, 2004 , vol. 45, # 25 p. 4989 - 4992
