sodium hydride in N,N-dimethyl-formamide
T=170°C; 15 h; Inert atmosphere;
参考文献
Park, Young Sue; Park, Sang Jun; Shin, Woong; Lee, Bong; Jung, Bumsuk; Kim, Joo Hyun
Molecular Crystals and Liquid Crystals, 2011 , vol. 538, p. 118 - 126
1: (methoxymethyl)-triphenylphosphonium chloride With phenyllithium in tetrahydrofuran
T=0°C; Dehydrochlorination; 0.166667 h;
2: 4-fluorobenzenecarbonitrile in tetrahydrofuran
T=20°C; Alkylation; 2 h;
3: With water in tetrahydrofuran
Hydrolysis;
