potassium carbonate in dimethyl sulfoxide
T=90°C; 8 h;
参考文献
Tangallapally, Rajendra P.; Yendapally, Raghunandan; Lee, Robin E.; Lenaerts, Anne J. M.; Lee, Richard E.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 26 p. 8261 - 8269
potassium carbonate in dimethyl sulfoxide
T=90°C; 8 h;
参考文献
THE UNIVERSITY OF TENNESSEE RESEARCH FOUNDATION; COLORADO STATE UNIVERSITY RESEARCH FOUNDATION
Patent: WO2005/7625 A2, 2005 ;
Location in patent: Page 63 ;
1: potassium hydroxide / N,N-dimethyl-formamide / 0.33 h / 175 °C / |Sealed tube
2: potassium hydroxide; sulfuric acid; acetic acid / water / |Reflux
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参考文献
Kormos, Chad M.; Jin, Chunyang; Cueva, Juan Pablo; Runyon, Scott P.; Thomas, James B.; Brieaddy, Lawrence E.; Mascarella, S. Wayne; Navarro, Hernan A.; Gilmour, Brian P.; Carroll, F. Ivy
Journal of Medicinal Chemistry, 2013 , vol. 56, # 11 p. 4551 - 4567
