反应条件
1: 1.) O3, 2.) NaI / 1.) MeOH, CH2Cl2, -73 deg C, 5 h, 2.) MeOH, CH2Cl2, AcOH, 0 deg C, 15 min, and room temperature, 1 h 2: 5.08 g / m-chloroperbenzoic acid / CH2Cl2 / 96 h / Ambient temperature 3: Jones reagent / acetone / 0.83 h / Ambient temperature 4: 3.47 g / p-TsOH*H2O / benzene / 2 h / Heating 5: hydrogen / 2percent Pd/SrCO3 / ethanol View Scheme
参考文献
Tanaka, Akira; Kamata, Hirotoshi; Yamashita, Kyohei
Agricultural and Biological Chemistry, 1988 , vol. 52, # 8 p. 2043 - 2048
