(+)-对-薄荷-1-烯合成路线 （共 31 条）
反应条件
ethanol; lithium; nickel dichloride; 4,4'-di-tert-butylbiphenyl in tetrahydrofuran T=20°C; 22 h;
参考文献
Alonso, Francisco; Osante, Inaki; Yus, Miguel
Tetrahedron, 2007 , vol. 63, # 1 p. 93 - 102
反应条件
(1,2-bis(diphenylphosphino)ethane)CoNs2; hydrogen in benzene T=25°C; P=3040.2 Torr; 6 h; Time;
参考文献
Kitahara, Takeshi; Mori, Masataka; Mori, Kenji
Tetrahedron, 1987 , vol. 43, # 12 p. 2689 - 2700
反应条件
hydrogen; lt;bis(dimethylsilyltetramethylcyclopentadienyl)NdHgt;2 in neat (no solvent)
参考文献
Jeske, Gerald; Lauke, Harald; Mauermann, Heiko; Schumann, Herbert; Marks, Tobin J.
Journal of the American Chemical Society, 1985 , vol. 107, # 26 p. 8111 - 8118
反应条件
C30H44FeN3; hydrogen in benzene T=20°C; 24 h; Inert atmosphere;
参考文献
Sabatier; Senderens
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1902 , vol. 134, p. 1127
反应条件
hydrogen; triphenylphosphine; tin(ll) chloride; PtCl2*1,4-bis(diphenylphosphyno)propane in benzene T=130°C; P=67505.4 Torr; 50 h; Further byproducts given;
参考文献
Dias, Adelson de O.; Augusti, Rodinei; Dos Santos, Eduardo N.; Gusevskaya, Elena V.
Tetrahedron Letters, 1997 , vol. 38, # 1 p. 41 - 44
反应条件
ammonia; lithium in tetrahydrofuran 1) -78 deg C, 0.5h, 2) reflux;
参考文献
Vaillancourt, Valerie; Agharahimi, Mohamad R.; Sundram, Uma N.; Richou, Olivier; Faulkner, D. John; Albizati, Kim F.
Journal of Organic Chemistry, 1991 , vol. 56, # 1 p. 378 - 387
反应条件
hydrogen; triphenylphosphine; tin(ll) chloride; (1,4-bis(diphenylphosphanyl)butane)dichloridoplatinum(II) in benzene T=130°C; P=67505.4 Torr; 50 h; Further byproducts given;
参考文献
Dias, Adelson de O.; Augusti, Rodinei; Dos Santos, Eduardo N.; Gusevskaya, Elena V.
Tetrahedron Letters, 1997 , vol. 38, # 1 p. 41 - 44
反应条件
nickel dichloride; zinc in methanol; 2-methoxy-ethanol T=50°C; 13 h;
参考文献
Schneider, David F; Viljoen, Murray S
Tetrahedron, 2002 , vol. 58, # 26 p. 5307 - 5315
反应条件
sodium naphthaleimide in tetrahydrofuran T=-78°C; 0.25 h;
参考文献
Vaillancourt, Valerie; Agharahimi, Mohamad R.; Sundram, Uma N.; Richou, Olivier; Faulkner, D. John; Albizati, Kim F.
Journal of Organic Chemistry, 1991 , vol. 56, # 1 p. 378 - 387
反应条件
1: 69 percent / Br, HOAc / 6 h / 80 °C 2: 63 percent / Br2, chlorosulfonic acid / 5 h / 25 °C 3: 60 percent / Zn, HOAc / 2 h / 25 °C 4: 1) sodium naphthaleimide / 1) THF, -78 deg C, 15 min 5: 80 percent / Li, NH3 / tetrahydrofuran / 1) -78 deg C, 0.5h, 2) reflux View Scheme
参考文献
Vaillancourt, Valerie; Agharahimi, Mohamad R.; Sundram, Uma N.; Richou, Olivier; Faulkner, D. John; Albizati, Kim F.
Journal of Organic Chemistry, 1991 , vol. 56, # 1 p. 378 - 387
