1-甲基-4-(1-甲基乙烯基)苯合成路线 (共 150 条)
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene T=65°C; 1 h;
参考文献
Saito, Shinichi; Salter, Matthew M.; Gevorgyan, Vladimir; Tsuboya, Norie; Tando, Kazushi; Yamamoto, Yoshinori
Journal of the American Chemical Society, 1996 , vol. 118, # 16 p. 3970 - 3971
反应条件
nitrogen trifluoride T=385 - 425°C; P=760.051 Torr; Inert atmosphere;
参考文献
Journal of Fluorine Chemistry, , vol. 132, # 5 p. 318 - 322
反应条件
1: Methyltriphenylphosphonium bromide With potassium tert-butylate in tetrahydrofuran T=0°C; 0.75 h; Inert atmosphere; 2: para-methylacetophenone in tetrahydrofuran T=0 - 20°C; 16 h; Inert atmosphere;
参考文献
Tripathi, Chandra Bhushan; Mukherjee, Santanu
Angewandte Chemie - International Edition, 2013 , vol. 52, # 32 p. 8450 - 8453
Angew. Chem., 2013 , vol. 125, # 32 p. 8608 - 8611,4
反应条件
(iPr)CuCl; triphenylphosphine; isopropyl alcohol in tetrahydrofuran; diethyl ether T=60°C; 16 h;
参考文献
Lebel, Helene; Davi, Michael; Diez-Gonzalez, Silvia; Nolan, Steven P.
Journal of Organic Chemistry, 2007 , vol. 72, # 1 p. 144 - 149
反应条件
nitrogen(IV) oxide T=-78°C; 2 h; Irradiation;
参考文献
Bosch, E.; Kochi, J. K.
Journal of Organic Chemistry, 1994 , vol. 59, # 12 p. 3314 - 3325
反应条件
[NiI2(PPh3)]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=70°C; Kumada Cross-Coupling; Inert atmosphere; chemoselective reaction;
参考文献
Wu, Ji-Cheng; Gong, Lu-Bing; Xia, Yuanzhi; Song, Ren-Jie; Xie, Ye-Xiang; Li, Jin-Heng
Angewandte Chemie - International Edition, 2012 , vol. 51, # 39 p. 9909 - 9913
反应条件
[NiI2(PPh3)]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=70°C; Kumada Cross-Coupling; Inert atmosphere;
参考文献
Wu, Ji-Cheng; Gong, Lu-Bing; Xia, Yuanzhi; Song, Ren-Jie; Xie, Ye-Xiang; Li, Jin-Heng
Angewandte Chemie - International Edition, 2012 , vol. 51, # 39 p. 9909 - 9913
反应条件
potassium hydrogensulfate T=100 - 200°C; P=100 Torr;
参考文献
Gharpure, M. M.; Joshi, P. L.; Rao, A. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 1214 - 1215
反应条件
carbon dioxide T=625°C; Leiten ueber Vanadin(V)-oxyd auf Aluminiumoxyd;
参考文献
Doklady Akademii Nauk SSSR, , vol. 41, p. 71
Doklady Akademii Nauk SSSR, , vol. 41, p. 67
Chem.Abstr., , p. 5206
反应条件
[Pd(1,3-bis(2,6-bis(diphenylmethyl)-4-methylphenyl)imidazol-2-ylidene)(cinnamyl)Cl] in tetrahydrofuran; 1,4-dioxane T=20°C; Kumada Cross-Coupling; 12 h; Inert atmosphere;
参考文献
Bastug, Gulluzar; Nolan, Steven P.
Organometallics, 2014 , vol. 33, # 5 p. 1253 - 1258