1-甲基-4-(1-甲基乙烯基)苯合成路线 （共 150 条）
反应条件
n-butyllithium; potassium 2-methyl-2-butoxide 1) r.t., 17 h, 2) reflux, 6 h; further reagent: D2O; Mechanism;
参考文献
Wilhelm, Dieter; Clark, Timothy; Friedl, Thomas; Schleyer, Paul von Rague
Chemische Berichte, 1983 , vol. 116, # 2 p. 751 - 760
反应条件
air; citric acid in ethanol T=38°C; 48 h; other times; also for geranial, citral; investigation of the deterioration mechanism for citral;
参考文献
Agricultural and Biological Chemistry, , vol. 46, # 5 p. 1387 - 1390
反应条件
chlorine in tetrachloromethane 0.0833333 h; Photolysis;
参考文献
Russian Journal of Organic Chemistry, , vol. 37, # 2 p. 270 - 280
参考文献
Chemische Berichte, , vol. 45, p. 2279
反应条件
platinum on activated charcoal T=180 - 200°C; incomplete reaction; Further byproducts given. Title compound not separated from byproducts;
参考文献
Manukov, E. N.; Chuiko, V. A.; Vyglazov, O. G.
Chemistry of Natural Compounds, 1982 , vol. 18, # 2 p. 242
Khimiya Prirodnykh Soedinenii, 1982 , # 2 p. 259 - 260
反应条件
1: 1.) pyridine, SOCl2, 2.) DBN / 1.) CH2Cl2, RT, 6 h, 2.) benzene, reflux, 5 h 2: 1.) n-BuLi / 1.) THF, 2.) THF, RT, 4 h View Scheme
参考文献
Synthetic Communications, , vol. 22, # 11 p. 1603 - 1609
反应条件
T=350 - 625°C; Leiten ueber Chrom(III)-oxyd auf Aluminiumoxyd;
反应条件
dimethylaluminum chloride in dichloromethane 3 h; influence of catalysis, solvent, time of reaction; Product distribution;
参考文献
Synthetic Communications, , vol. 17, # 10 p. 1217 - 1226
反应条件
pyridine in acetonitrile T=24°C; Kinetics; Further Variations:Temperatures;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 44, # 8 p. 1731 - 1734
反应条件
1: copper (II)-formate; nickel-formate / 175 °C 2: manganese (II)-acetate; lead (II)-acetate / 45 °C / Einleiten von Luft 3: charcoal / 53 Torr View Scheme
参考文献
Industrial and Engineering Chemistry, , vol. 34, p. 1028,1032
