1-氯-4-(甲氧基甲基)苯合成路线 （共 28 条）
反应条件
in water; acetonitrile
T=75°C;
参考文献
Bentley, T. William; Koo, In Sun; Choi, Hojune; Llewellyn, Gareth
Journal of Physical Organic Chemistry, 2008 , vol. 21, # 3 p. 251 - 256
反应条件
sulfuric acid; tetraethylammonium p-toluenesulfonate
1.) electrochemical anodic oxidation, AcOH, 2.) RT, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Nishiguchi, Ikuzo; Hirashima, Tsuneaki
Journal of Organic Chemistry, 1985 , vol. 50, # 4 p. 539 - 541
反应条件
in dimethylsulfoxide-d6
T=30.3°C; Rate constant;
参考文献
Fountain; White, Robert D.; Patel, Kamlesh D.; New, Dallas G.; Xu, YuBo; Cassely, Aaron J.
Journal of Organic Chemistry, 1996 , vol. 61, # 26 p. 9434 - 9436
反应条件
2,6-dimethylpyridine
T=32°C; Rate constant;
参考文献
Braverman, Samuel; Manor, Haim
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 53, # 1-4 p. 357 - 365
反应条件
pyridine; sodium in methanol
5 h; Irradiationelectrochemical oxidation in absence and presence of ultrasound; Product distribution;
参考文献
Walton, D.J.; Chyla, A.; Lorimer, J.P.; Mason, T.J.
Synthetic Communications, 1990 , vol. 20, # 12 p. 1843 - 1852
反应条件
Ambient temperatureIrradiationrelative yields of products for different substituents;
参考文献
Tomioka, Hideo; Tabayashi, Kazuo; Ozaki, Yasuji; Izawa, Yasuji
Tetrahedron, 1985 , vol. 41, # 8 p. 1435 - 1440
反应条件
48 h; Irradiationvarious substituted p-chlorotoluenes under different conditions; acetone as sensitizer; Product distribution;
参考文献
Choudhry, Ghulam Ghaus; Roof, Antonius Aloysius Maria; Hutzinger, Otto
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 12 p. 2957 - 2962
反应条件
1: 1-chloro-4-(methoxymethyl)benzene With 2,3-dicyano-5,6-dichloro-p-benzoquinone; bis-[(trifluoroacetoxy)iodo]benzene in 1,2-dichloro-ethane
T=80°C; 3 h; Inert atmosphere;
2: PhMgI in diethyl ether; 1,2-dichloro-ethane
T=-20°C; 3 h; Inert atmosphere;
参考文献
Muramatsu, Wataru; Nakano, Kimihiro
Organic Letters, 2014 , vol. 16, # 7 p. 2042 - 2045
