2-溴-5,5-二甲基-1,3-环己二酮合成路线 （共 36 条）
反应条件
chloroform
durch Chlorierung;
参考文献
Voitila <Fjaeder>
Annales Academiae Scientiarum Fennicae, Series A, 1937 , vol. 49, # 1 p. 79 Anm. 1
反应条件
bei der Chlorierung;
参考文献
Norris; Thorpe
Journal of the Chemical Society, 1921 , vol. 119, p. 1206
反应条件
in ethanol
0.25 h; Heating;
参考文献
Schank, Kurt; Buegler, Stephan; Folz, Harald; Schott, Norbert
Helvetica Chimica Acta, 2007 , vol. 90, # 8 p. 1606 - 1649
反应条件
1.1: 97 percent / AcONa / H2O / 0 °C
2.1: aq. NaOH / 0.5 h / 40 - 50 °C
2.2: 83 percent / aq. HCl / pH 2 - 3
3.1: 85 percent / aq. ethanol / 0.25 h / Heating
View Scheme
参考文献
Schank, Kurt; Buegler, Stephan; Folz, Harald; Schott, Norbert
Helvetica Chimica Acta, 2007 , vol. 90, # 8 p. 1606 - 1649
反应条件
1.1: 97 percent / AcONa / H2O / 0 °C
2.1: aq. NaOH / 0.5 h / 40 - 50 °C
2.2: 83 percent / aq. HCl / pH 2 - 3
3.1: 92 percent / aq. NaOH; O2
View Scheme
参考文献
Schank, Kurt; Buegler, Stephan; Folz, Harald; Schott, Norbert
Helvetica Chimica Acta, 2007 , vol. 90, # 8 p. 1606 - 1649
反应条件
piperidine in ethanol
0.05 h; microwave irradiation;
参考文献
Dabholkar, Vijay V.; Mishra, Sushil Kumar J.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 9 p. 2112 - 2117
