2,2,6,6-四甲基环己酮合成路线 （共 45 条）
反应条件
oxygen in dichloromethane
T=22°C; 2 h; Irradiationdye-sensitized oxidation;
参考文献
Rao, V. Jayathirtha; Ramamurthy, V.; Schaumann, E.; Nimmesgern, H.
Journal of Organic Chemistry, 1984 , vol. 49, # 4 p. 615 - 621
反应条件
oxygen in methanol
T=22°C; 2 h; Irradiationdye-sensitized oxidation;
参考文献
Rao, V. Jayathirtha; Ramamurthy, V.; Schaumann, E.; Nimmesgern, H.
Journal of Organic Chemistry, 1984 , vol. 49, # 4 p. 615 - 621
反应条件
diethyl ether; sodium amide
参考文献
Sobotka; Chanley
Journal of the American Chemical Society, 1949 , vol. 71, p. 4136,4138
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Colonge
Bulletin de la Societe Chimique de France, 1938 , vol. <5> 5, p. 98
反应条件
Sodium bromate; sodium hydrogensulfite in water; acetonitrile
T=21°C; pH=1.7; 2 h;
参考文献
Bierenstiel, Matthias; D'Hondt, Paul J.; Schlaf, Marcel
Tetrahedron, 2005 , vol. 61, # 21 p. 4911 - 4917
反应条件
ozone in diethyl ether
T=-70°C;
参考文献
Kawamura, Shin-Ichi; Yamakoshi, Hideyuki; Abe, Manabu; Masuyama, Araki; Nojima, Masatomo
Tetrahedron, 2002 , vol. 58, # 5 p. 891 - 896
反应条件
potassium hydroxide; DC-18-C-6 in toluene
T=50°C; 5 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Artaud, I.; Torossian, G.; Viout, P.
Tetrahedron, 1985 , vol. 41, # 21 p. 5031 - 5038
反应条件
potassium hydroxide; DC-18-C-6 in toluene
T=50°C; 5 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Artaud, I.; Torossian, G.; Viout, P.
Tetrahedron, 1985 , vol. 41, # 21 p. 5031 - 5038
反应条件
potassium hydroxide; DC-18-C-6 in toluene
T=50°C; 5 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Artaud, I.; Torossian, G.; Viout, P.
Tetrahedron, 1985 , vol. 41, # 21 p. 5031 - 5038
反应条件
potassium hydroxide; DC-18-C-6 in toluene
T=50°C; 5 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Artaud, I.; Torossian, G.; Viout, P.
Tetrahedron, 1985 , vol. 41, # 21 p. 5031 - 5038
反应条件
lithium diisopropyl amide
1) THF, a) -78 deg C, 1 h, b) 0 deg C, 1 h, 2) 0 deg C, 20 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kutney, James P.; Gunning, Philip J.; Clewley, Robin G.; Somerville, John; Rettig, Steven J.
Canadian Journal of Chemistry, 1992 , vol. 70, # 7 p. 2094 - 2114
