(2-异氰基-2-丙基)苯合成路线 （共 7 条）
反应条件
4-methyl-morpholine; trichloromethyl chloroformate in dichloromethane T=-30°C; 1 h;
参考文献
Kamer, Paul C. J.; Nolte, Roeland J. M.; Drenth, Wiendelt
Journal of the American Chemical Society, 1988 , vol. 110, # 20 p. 6818 - 6825
反应条件
1: 75 percent / Et3N; 4-(dimethylamino)pyridine / tetrahydrofuran / 2 h / 20 °C 2: 33 percent / 2,6-dimethyl-1,4-benzoquinone / CH2Cl2 / 12 h / 20 °C View Scheme
参考文献
Kamer, Paul C. J.; Nolte, Roeland J. M.; Drenth, Wiendelt
Journal of the American Chemical Society, 1988 , vol. 110, # 20 p. 6818 - 6825
反应条件
1: 53 percent / liquid ammonia 3: 96 percent / N-methylmorpholine, diphosgene / CH2Cl2 / 1 h / -30 °C View Scheme
参考文献
Kamer, Paul C. J.; Nolte, Roeland J. M.; Drenth, Wiendelt
Journal of the American Chemical Society, 1988 , vol. 110, # 20 p. 6818 - 6825
反应条件
2: 96 percent / N-methylmorpholine, diphosgene / CH2Cl2 / 1 h / -30 °C View Scheme
参考文献
Kamer, Paul C. J.; Nolte, Roeland J. M.; Drenth, Wiendelt
Journal of the American Chemical Society, 1988 , vol. 110, # 20 p. 6818 - 6825
反应条件
2,6-dimethyl-1,4-benzoquinone in dichloromethane T=20°C; 12 h;
参考文献
Masutani, Kouta; Minowa, Tomofumi; Hagiwara, Yoshiaki; Mukaiyama, Teruaki
Bulletin of the Chemical Society of Japan, 2006 , vol. 79, # 7 p. 1106 - 1117
反应条件
T=520 - 550°C; P=0.01 Torr;
参考文献
Chemische Berichte, , vol. 120, p. 1 - 4
反应条件
T=520 - 550°C; P=0.01 Torr;
参考文献
Chemische Berichte, , vol. 120, p. 1 - 4
