N-(4-硝基苯基)二十碳-5,8,11,14-四烯酰胺合成路线 （共 6 条）
反应条件
1: oxalyl chloride, DMF / benzene / Ambient temperature 2: tetrahydrofuran View Scheme
参考文献
Barton, Derek H. R.; Ozbalik, Nubar; Vacher, Bernard
Tetrahedron, 1988 , vol. 44, # 12 p. 3501 - 3512
反应条件
1: 3 N aq. NaOH / ethanol / 12 h / Ambient temperature 2: oxalyl chloride, DMF / benzene / Ambient temperature 3: tetrahydrofuran View Scheme
参考文献
Barton, Derek H. R.; Ozbalik, Nubar; Vacher, Bernard
Tetrahedron, 1988 , vol. 44, # 12 p. 3501 - 3512
反应条件
in benzene T=40°C; 1 h; Irradiation(13)C-labelling study; Mechanism;
参考文献
Barton, Derek H. R.; Ozbalik, Nubar; Vacher, Bernard
Tetrahedron, 1988 , vol. 44, # 12 p. 3501 - 3512
参考文献
Barton, Derek H. R.; Ozbalik, Nubar; Vacher, Bernard
Tetrahedron, 1988 , vol. 44, # 12 p. 3501 - 3512
反应条件
1: 1.) phosgene, 2.) pyridine / 1.) CH2Cl2, 0 deg C, 2.) CH2Cl2, rt, 30 min, 3.) CH2Cl2, 3 h 2: 3 N aq. NaOH / ethanol / 12 h / Ambient temperature View Scheme
参考文献
Barton, Derek H. R.; Ozbalik, Nubar; Vacher, Bernard
Tetrahedron, 1988 , vol. 44, # 12 p. 3501 - 3512
反应条件
1: 1.) phosgene, 2.) pyridine / 1.) CH2Cl2, 0 deg C, 2.) CH2Cl2, rt, 30 min, 3.) CH2Cl2, 3 h
2: 3 N aq. NaOH / ethanol / 12 h / Ambient temperature
3: oxalyl chloride, DMF / benzene / Ambient temperature
View Scheme
参考文献
Barton, Derek H. R.; Ozbalik, Nubar; Vacher, Bernard
Tetrahedron, 1988 , vol. 44, # 12 p. 3501 - 3512
