1-(2-羟基苯基)-1-乙酮肟合成路线 (共 21 条)
反应条件
hydroxylamine hydrochloride; sodium acetate in ethanol Condensation; 0.05 h; Irradiation;
参考文献
Mitra, Alok Kumar; De, Aparna; Karchaudhuri, Nilay
Journal of the Indian Chemical Society, 1999 , vol. 76, # 4 p. 218 - 219
反应条件
methanecarbohydroxamic acid; sulfuric acid in acetonitrile T=80°C; P=1292.9 Torr; 0.133333 h; Microwave irradiation;
参考文献
Tetrahedron Letters, , vol. 52, # 46 p. 6103 - 6107
反应条件
sodium azide; trifluoroacetic acid in methanol T=5°C; 11 h;
参考文献
Adam; Hadjiarapoglou; Mosandl; Saha-Moeller; Wild
Journal of the American Chemical Society, 1991 , vol. 113, # 21 p. 8005 - 8011
反应条件
hydrogenchloride; zinc in ethanol; water 40 h; Heating;
参考文献
Boulton, A. J.; Tsoungas, Petros G.; Tsiamis, Chris
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 695 - 698
反应条件
methanol; hydroxylamine hydrochloride; sodium methylate 5 - 10 h; Heating / reflux;
参考文献
WO2005/44808 A1, ;
Page/Page column 9 ;
反应条件
methanecarbohydroxamic acid; sulfuric acid in acetonitrile 10 h; Reflux;
参考文献
Tetrahedron Letters, , vol. 52, # 46 p. 6103 - 6107
反应条件
1: ZnCl2 / 125 °C View Scheme
参考文献
Journal of the Chemical Society, , p. 280,291
反应条件
1: ZnCl2 View Scheme
参考文献
Journal of the Chemical Society, , p. 280,291
反应条件
trifluoromethylsulfonic anhydride in dichloromethane T=20°C; 5 h; Inert atmosphere;
参考文献
Kalkhambkar, Rajesh G.; Yuvaraj
Synthetic Communications, 2014 , vol. 44, # 4 p. 547 - 555
反应条件
trichloromethylcarbonyl isocyanate in tetrahydrofuran 0.166667 h; Ambient temperature;
参考文献
Stokker, Gerald
Journal of Organic Chemistry, 1983 , vol. 48, # 15 p. 2613 - 2615