1-(2-羟基苯基)-1-乙酮肟合成路线 （共 21 条）
反应条件
HY-Zeolite in benzene T=160°C; 168 h;
参考文献
Synthetic Communications, , vol. 25, # 21 p. 3315 - 3321
反应条件
trichloromethylcarbonyl isocyanate in tetrahydrofuran 0.166667 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 48, # 15 p. 2613 - 2615
反应条件
propane-1,2,3-tricarboxylic acid T=160°C; Beckmann rearrangement; 0.0833333 h; Inert atmosphereneat (no solvent);
参考文献
Thopate, Shankar Ramchandra; Kote, Santosh Rajaram; Rohokale, Sandeep Vasantrao; Thorat, Nitin Madhukar
Journal of Chemical Research, 2011 , vol. 35, # 2 p. 124 - 125
反应条件
periodic acid T=20°C; 0.0666667 h;
参考文献
Li, Zheng; Ding, Run-Bo; Xing, Yu-Lin; Shi, Sheng-Yi
Synthetic Communications, 2005 , vol. 35, # 19 p. 2515 - 2520
参考文献
v.Auwers; Lechner; Bundesmann
Chemische Berichte, 1925 , vol. 58, p. 41
反应条件
indium trifluoromethanesulfonate in acetonitrile
Beckmann rearrangement; 2.5 h; Heating;
参考文献
Barman, Dhiren C.; Gohain, Mukut; Prajapati, Dipak; Sandhu, Jagir S.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002 , vol. 41, # 1 p. 154 - 156
反应条件
N-chloro-succinimide; sodium hydroxide in water
T=20°C;
参考文献
Kociolek, Martin G.; Hoermann, Olivia
Synthetic Communications, 2012 , vol. 42, # 17 p. 2632 - 2638
反应条件
1: 67 percent / diethyl ether / 1.) -70 grad C, 2 h, 2.) 0 grad C, 4 h, 3.) room temperature, 3 days
2: aq. NaOH
View Scheme
参考文献
Bonsignore, Leonardo; Loy, Guiseppe; Secci, Mario
Tetrahedron Letters, 1983 , vol. 24, # 45 p. 5013 - 5016
反应条件
in diethyl ether
1.) -70 grad C, 2 h, 2.) 0 grad C, 4 h, 3.) room temperature, 3 days;
参考文献
Bonsignore, Leonardo; Loy, Guiseppe; Secci, Mario
Tetrahedron Letters, 1983 , vol. 24, # 45 p. 5013 - 5016
参考文献
Lovering, Frank; Kirincich, Steve; Wang, Weiheng; Combs, Kerry; Resnick, Lynn; Sabalski, Joan E.; Butera, John; Liu, Julie; Parris, Kevin; Telliez
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 9 p. 3342 - 3351
