3,4-二氢异喹啉-1(2H)-酮合成路线 （共 71 条）
反应条件
trifluorormethanesulfonic acid T=50°C; Inert atmosphere;
参考文献
Board of Trustees of Northern Illinois University; Klumpp, Douglas A.; Raja, Erum K.
Patent: US2013/267712 A1, 2013 ;
Location in patent: Paragraph 0041-0042 ;
反应条件
trifluorormethanesulfonic acid in dichloromethane T=50°C; 12 h;
参考文献
Board of Trustees of Northern Illinois University; Klumpp, Douglas A.; Raja, Erum K.
Patent: US2013/267712 A1, 2013 ;
Location in patent: Paragraph 0046 ;
反应条件
phosphorus pentoxide; trichlorophosphate 2 h; Heating;
参考文献
Decker, Michael
European Journal of Medicinal Chemistry, 2005 , vol. 40, # 3 p. 305 - 313
反应条件
tetrabutylammomium bromide; dicobalt octacarbonyl in sodium hydroxide; benzene T=65°C; 5.5 h; Irradiation;
参考文献
Brunet, Jean-Jacques; Sidot, Christian; Caubere, Paul
Journal of Organic Chemistry, 1983 , vol. 48, # 8 p. 1166 - 1171
反应条件
sodium hydroxide in water T=90°C; 24 h;
参考文献
Preedasuriyachai, Patcharee; Chavasiri, Warinthorn; Sakurai, Hidehiro
Synlett, 2011 , # 8 art. no. U00511ST, p. 1121 - 1124
反应条件
[{(η5-C5Me5)RhCl}2(μ-Cl)2]; caesium acetate in methanol T=20°C; 16 h;
参考文献
Guimond, Nicolas; Gorelsky, Serge I.; Fagnou, Keith
Journal of the American Chemical Society, 2011 , vol. 133, # 16 p. 6449 - 6457
反应条件
potassium hydroxide; dihydrogen peroxide in methanol; water 0.5 h; Ambient temperature;
参考文献
Girard; Atkinson; Belanger; et al.
Journal of Organic Chemistry, 1983 , vol. 48, # 19 p. 3220 - 3234
参考文献
Smithkline Beecham Corporation
Patent: US5602145 A1, 1997 ;
反应条件
trifluorormethanesulfonic acid in dichloromethane T=0°C; 1 h; Inert atmosphere;
参考文献
Kurouchi, Hiroaki; Kawamoto, Kyoko; Sugimoto, Hiromichi; Nakamura, Satoshi; Otani, Yuko; Ohwada, Tomohiko
Journal of Organic Chemistry, 2012 , vol. 77, # 20 p. 9313 - 9328,16
反应条件
1: With sodium chlorite; sodium dihydrogenphosphate in tetrahydrofuran; water T=20°C; Pinnick oxidation; 2: With sodium hyposulfite in tetrahydrofuran; water; ethyl acetate T=20°C;
参考文献
Mohamed, Magdi A.; Yamada, Ken-ichi; Tomioka, Kiyoshi
Tetrahedron Letters, 2009 , vol. 50, # 26 p. 3436 - 3438
