3,4-二氢异喹啉-1(2H)-酮合成路线 (共 71 条)
反应条件
in acetone Ambient temperature;
参考文献
Rozwadowska, Maria; Brozda, Danuta
Canadian Journal of Chemistry, 1980 , vol. 58, p. 1239 - 1242
反应条件
1: AlCl3 / CH2Cl2 / -40 - 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 11, # 10 p. 2205 - 2209
反应条件
1: TosN3; TEA / acetonitrile 2: 72 percent / Rh2(OAc)4 / toluene / Heating 3: H2O View Scheme
参考文献
Tetrahedron Letters, , vol. 40, # 47 p. 8269 - 8270
反应条件
1: 72 percent / Rh2(OAc)4 / toluene / Heating 2: H2O View Scheme
参考文献
Tetrahedron Letters, , vol. 40, # 47 p. 8269 - 8270
反应条件
1: trifluoroacetic acid / dichloromethane 2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 60 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 3 p. 656 - 658
反应条件
1: triethylamine / tetrahydrofuran / 6 h / 20 °C 2: [{(η5-C5Me5)RhCl}2(μ-Cl)2]; caesium acetate / methanol / 16 h / 60 °C / 3750.38 Torr / Autoclave View Scheme
参考文献
Journal of the American Chemical Society, , vol. 133, # 8 p. 2350 - 2353
反应条件
bismuth trifluoromethanesulphonate T=100 - 120°C; Beckmann rearrangement; 0.5 h; Title compound not separated from byproducts;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 12, # 3 p. 387 - 390
反应条件
hydrogenchloride; potassium iodide; sodium nitrite 1) H2O, 0 degC, 1.5 h, 2) warm to room temp., 4 h; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Girard; Atkinson; Belanger; et al.
Journal of Organic Chemistry, 1983 , vol. 48, # 19 p. 3220 - 3234
反应条件
oxygen; methylene blue in chloroform 60 h; Ambient temperatureIrradiation;
参考文献
Tetrahedron Letters, , vol. 21, p. 2613 - 2616
反应条件
ethanol; nickel; ethyl acetate Hydrogenation;
参考文献
Archiv der Pharmazie (Weinheim, Germany), , vol. 291, p. 560,565