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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1196154-02-5
合成路线
(共 4 条)
1352934-60-1
→
反应条件
1196154-02-5
反应条件
trichlorophosphate T=150°C; 18 h;
参考文献
Subasinghe, Nalin L.; Lanter, James; Markotan, Thomas; Opas, Evan; McKenney, Sandra; Crysler, Carl; Hou, Cuifen; O'Neill, John; Johnson, Dana; Sui, Zhihua
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 4 p. 1063 - 1069
215453-51-3
7-溴-1-氯异喹啉
→
反应条件
1196154-02-5
反应条件
1.1: n-butyllithium / tetrahydrofuran / 0.25 h / -78 °C 1.2: -78 - 20 °C 2.1: copper / N,N-dimethyl-formamide / 48 h / 80 °C 3.1: trichlorophosphate / 18 h / 150 °C View Scheme
参考文献
Subasinghe, Nalin L.; Lanter, James; Markotan, Thomas; Opas, Evan; McKenney, Sandra; Crysler, Carl; Hou, Cuifen; O'Neill, John; Johnson, Dana; Sui, Zhihua
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 4 p. 1063 - 1069
1170704-54-7
→
反应条件
1196154-02-5
反应条件
1: copper / N,N-dimethyl-formamide / 48 h / 80 °C 2: trichlorophosphate / 18 h / 150 °C View Scheme
参考文献
Subasinghe, Nalin L.; Lanter, James; Markotan, Thomas; Opas, Evan; McKenney, Sandra; Crysler, Carl; Hou, Cuifen; O'Neill, John; Johnson, Dana; Sui, Zhihua
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 4 p. 1063 - 1069
1196154-02-5
→
反应条件
1196147-73-5
反应条件
1: potassium hydroxide / 72 h / 100 °C 2: ammonium acetate / 4 h / 160 °C View Scheme
参考文献
Subasinghe, Nalin L.; Lanter, James; Markotan, Thomas; Opas, Evan; McKenney, Sandra; Crysler, Carl; Hou, Cuifen; O'Neill, John; Johnson, Dana; Sui, Zhihua
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 4 p. 1063 - 1069