乙基4-乙酰基-1H-吡咯-2-羧酸酯合成路线 （共 9 条）
反应条件
aluminium trichloride in 1,2-dichloro-ethane 1 h; Ambient temperature;
参考文献
Tani; Ariyasu; Nishiyama; Hagiwara; Watanabe; Yokoyama; Murakami
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 1 p. 48 - 54
反应条件
in ethanol T=0°C; 3.2 h;
参考文献
Tani; Ariyasu; Nishiyama; Hagiwara; Watanabe; Yokoyama; Murakami
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 1 p. 48 - 54
反应条件
aluminium trichloride in 1,2-dichloro-ethane T=0°C; 0.25 h;
参考文献
Tani; Ariyasu; Nishiyama; Hagiwara; Watanabe; Yokoyama; Murakami
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 1 p. 48 - 54
反应条件
1: 89 percent / AlCl3 / CH2Cl2; nitromethane / 3 h / -30 °C 2: 87 percent / ethanol / 20 °C View Scheme
参考文献
Tani; Ariyasu; Nishiyama; Hagiwara; Watanabe; Yokoyama; Murakami
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 1 p. 48 - 54
反应条件
boron trifluoride diethyl etherate in 1,2-dichloro-ethane T=0°C; 0.5 h; Yield given. Yields of byproduct given;
参考文献
Tani; Ariyasu; Nishiyama; Hagiwara; Watanabe; Yokoyama; Murakami
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 1 p. 48 - 54
反应条件
1: 78 percent / DBU / dimethylformamide / 6 h / 120 °C 2: 92 percent / Raney Ni / ethanol / 4 h / Heating View Scheme
参考文献
Misra; Panda; Ila; Junjappa
Journal of Organic Chemistry, 2007 , vol. 72, # 4 p. 1246 - 1251
反应条件
titanium tetrachloride in 1,2-dichloro-ethane 1 h; Ambient temperaturevarious Lewis-acids, temperatures, times; Product distribution;
参考文献
Murakami, Yasuoki; Tani, Masanobu; Ariyasu, Takahiro; Nishiyama, Chika; Watanabe, Toshiko; Yokoyama, Yuusaku
Heterocycles, 1988 , vol. 27, # 8 p. 1855 - 1860
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Tani; Ariyasu; Nishiyama; Hagiwara; Watanabe; Yokoyama; Murakami
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 1 p. 48 - 54
反应条件
1: 15percent aq. KOH / 1 h / 55 °C 2: Dowtherm-A / 6.3 h / 194 - 208 °C View Scheme
参考文献
Tani; Ariyasu; Nishiyama; Hagiwara; Watanabe; Yokoyama; Murakami
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 1 p. 48 - 54
反应条件
potassium hydroxide T=55°C; 1 h;
参考文献
Tani; Ariyasu; Nishiyama; Hagiwara; Watanabe; Yokoyama; Murakami
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 1 p. 48 - 54
