[6,13,20,27-四苯基-29H,31H-四苯并卟啉(2-)-kappa2N29,N31]钯合成路线 （共 3 条）
反应条件
in dichloromethane; N,N-dimethyl-formamide T=150°C; 0.75 h; Inert atmosphere;
参考文献
Cui, Xiaoneng; Zhao, Jianzhang; Yang, Pei; Sun, Jifu
Chemical Communications, 2013 , vol. 49, # 87 p. 10221 - 10223
反应条件
1: water / pH 3.0 2: melt / 1 h / 360 °C / |Inert atmosphere 3: hydrogenchloride / dichloromethane; water / 0.5 h 4: dichloromethane; N,N-dimethyl-formamide / 0.75 h / 150 °C / |Inert atmosphere View Scheme
参考文献
Chemical Communications, , vol. 49, # 87 p. 10221 - 10223
反应条件
1: sodium hydroxide / water / pH 8.0 2: water / pH 3.0 3: melt / 1 h / 360 °C / |Inert atmosphere 4: hydrogenchloride / dichloromethane; water / 0.5 h 5: dichloromethane; N,N-dimethyl-formamide / 0.75 h / 150 °C / |Inert atmosphere View Scheme
参考文献
Chemical Communications, , vol. 49, # 87 p. 10221 - 10223
