2-甲基-3-苯基-2-丙烯腈合成路线 （共 16 条）
参考文献
Pfeiffer; Engelhardt; Alfuss
Justus Liebigs Annalen der Chemie, 1928 , vol. 467, p. 171
反应条件
poly(N-isopropylacerylamide)-SCS-PdCl; TEA in n-heptane; N,N-dimethyl acetamide; water
T=95°C; Heck coupling; 10 h;
参考文献
Bergbreiter, David E.; Osburn, Philip L.; Wilson, Allan; Sink, Erin M.
Journal of the American Chemical Society, 2000 , vol. 122, # 38 p. 9058 - 9064
反应条件
ammonia; oxygen in tetrahydrofuran
T=120°C; P=4560.31 Torr; 5 h;
参考文献
Oishi, Takamichi; Yamaguchi, Kazuya; Mizuno, Noritaka
Angewandte Chemie, International Edition, 2009 , vol. 48, # 34 p. 6286 - 6288
Angewandte Chemie, 2009 , vol. 121, # 34 p. 6404 - 6406
反应条件
10 CuO-ZnO on activated carbon in toluene
T=100°C; 4 h; Inert atmosphere;
参考文献
Sharma, Sumeet K.; Bishopp, Simon D.; Liana Allen; Lawrence, Ruth; Bamford, Mark J.; Lapkin, Alexei A.; Plucinski, Pawel; Watson, Robert J.; Williams, Jonathan M.J.
Tetrahedron Letters, 2011 , vol. 52, # 33 p. 4252 - 4255
反应条件
sodium tetrahydroborate in methanol
T=20°C; 0.25 h;
参考文献
Das, Biswanath; Banerjee, Joydeep; Majhi, Anjoy; Mahender, Gurram
Tetrahedron Letters, 2004 , vol. 45, # 50 p. 9225 - 9227
反应条件
hydroxylamine hydrochloride; sodium iodide in acetonitrile
1.66667 h; Heating;
参考文献
Ballini, Roberto; Fiorini, Dennis; Palmieri, Alessandro
Synlett, 2003 , # 12 p. 1841 - 1843
反应条件
nickel sulphate; ammonium hydroxide; sodium hydroxide; dipotassium peroxodisulfate in water
6 h; Ambient temperature;
参考文献
Yamazaki, Shigakazu; Yamazaki, Yasuyuki
Chemistry Letters, 1990 , # 4 p. 571 - 574
反应条件
magnesium bromide in dichloromethane
Yield given;
参考文献
Okada, Hisashi; Matsuda, Isamu; Izumi, Yusuke
Chemistry Letters, 1983 , p. 97 - 100
反应条件
zinc(II) iodide in acetonitrile
Meerwein-type arylation;
参考文献
Patrick, Timothy B.; Juehne, Thomas; Reeb, Elmer; Hennessy, Daniel
Tetrahedron Letters, 2001 , vol. 42, # 21 p. 3553 - 3554
反应条件
1: 25 percent / acetic anhydride / 2 h / 60 °C
2: 70 percent / POCl3, diisopropylamine / CH2Cl2
3: 15 percent / 1.5 h / 540 °C / 0.01 Torr
View Scheme
参考文献
Meier, Michael; Ruechardt, Christoph
Chemische Berichte, 1987 , vol. 120, p. 1 - 4
