1197040-29-1合成路线 (共 99 条)
反应条件
hydrogenchloride; methanol; trimethylsilylazide in diethyl ether T=60°C; 5 h;
参考文献
Jin, Tienan; Kamijo, Shin; Yamamoto, Yoshinori
Tetrahedron Letters, 2004 , vol. 45, # 51 p. 9435 - 9437
反应条件
sodium tris(acetoxy)borohydride T=-40 - 0°C; 7 h; Further byproducts given;
参考文献
Kiselyov, Alexander S.
Tetrahedron Letters, 2005 , vol. 46, # 26 p. 4487 - 4490
反应条件
in hydrogen bromide 4 h; Heating;
参考文献
Shono, Tatsuya; Matsumura, Yoshihiro; Tsubata, Kenji
Tetrahedron Letters, 1981 , vol. 22, # 25 p. 2411 - 2412
反应条件
N-bromosuccinmide; sodium azide; [14C]-Tetramethylammonium bromide in chloroform; water 1.) 0 deg C, 5 min, 2.) 0 deg C, 45 min;
参考文献
Collibee; Nakajima; Anselme
Journal of Organic Chemistry, 1995 , vol. 60, # 2 p. 468 - 469
反应条件
hydrogenchloride; acetone
参考文献
Passerini
Gazzetta Chimica Italiana, 1927 , vol. 57, p. 454
反应条件
1: 46 percent / 576 h 2: 15percent H2SO4 / 1 h / Heating View Scheme
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 322, # 2 p. 273 - 280
反应条件
selenium; sulfur; triethylamine in tetrahydrofuran 2 h; Heating;
参考文献
Fujiwara, Shin-Ichi; Shin-Ike, Tsutomu; Sonoda, Noboru; Aoki, Minoru; Okada, Kazuhiro; Miyoshi, Noritaka; Kambe, Nobuaki
Tetrahedron Letters, 1991 , vol. 32, # 29 p. 3503 - 3506
反应条件
in tetrachloromethane 6 h; Reflux;
参考文献
Mendeleev Communications, , vol. 20, # 5 p. 282 - 284
反应条件
96 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Beckert, R.; Mayer, R.
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 2 p. 273 - 280
反应条件
96 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Beckert, R.; Mayer, R.
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 2 p. 273 - 280