1197040-29-1合成路线 （共 99 条）
反应条件
1: diethyl ether 2: alcoholic KOH-solution View Scheme
参考文献
Passerini
Gazzetta Chimica Italiana, 1923 , vol. 53, p. 413
参考文献
Grote,A. et al.
Justus Liebigs Annalen der Chemie, 1972 , vol. 755, p. 67 - 85
反应条件
1: 59 percent / benzene / 24 h / 100 °C 2: 68 percent / 0.25 h / 300 °C View Scheme
参考文献
Moderhack, Dietrich; Stolz, Karsten
Journal of Organic Chemistry, 1986 , vol. 51, # 5 p. 732 - 734
反应条件
N-chloro-succinimide; sodium azide; [14C]-Tetramethylammonium bromide in chloroform; water 1.) 0 deg C, 5 min, 2.) 0 deg C, 45 min;
参考文献
Collibee; Nakajima; Anselme
Journal of Organic Chemistry, 1995 , vol. 60, # 2 p. 468 - 469
反应条件
1: pyridine With fluorine in chloroform T=-78 - -60°C; 2: phenyl isocyanate With trimethylsilylazide in chloroform T=-50 - 0°C;
参考文献
Tetrahedron Letters, , vol. 46, # 29 p. 4851 - 4854
反应条件
1: pyridine With fluorine in dichloromethane T=-78 - -50°C; 2: phenyl isocyanate in dichloromethane T=-50 - 0°C; 4 h;
参考文献
Tetrahedron Letters, , vol. 46, # 13 p. 2279 - 2282
反应条件
1: pyridine With fluorine in chloroform T=-78 - -60°C; 2: diazoacetic acid ethyl ester; phenyl isocyanate in chloroform T=-60 - 20°C;
参考文献
Tetrahedron Letters, , vol. 47, # 15 p. 2631 - 2634
反应条件
sodium tris(acetoxy)borohydride T=-40 - 0°C; 7 h;
参考文献
Tetrahedron Letters, , vol. 46, # 26 p. 4487 - 4490
反应条件
sodium tris(acetoxy)borohydride T=-40 - 0°C; 7 h;
参考文献
Tetrahedron Letters, , vol. 46, # 26 p. 4487 - 4490
反应条件
1: pyridine With fluorine in dichloromethane T=-78 - -50°C; 2: phenyl isocyanate in dichloromethane T=-50 - 0°C; 4 h;
参考文献
Tetrahedron Letters, , vol. 46, # 13 p. 2279 - 2282
